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Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3 Job Number: C41950 Account: DECASM Dysert Environmental Project: Pactiv Packaging- 4545 Qantas Lane Stockton CA 95206 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch C41974-1MS L44731.D 1 09/28/15 XB n/a n/a VL1343 C41974-1MSD L44732.D 1 09/28/15 XB n/a n/a VL1343 C41974-1 L44725.D 1 09/28/15 XB n/a n/a VL1343 The QC reported here applies to the following samples: Method: SW846 8260B C41950-1 C41974-1 Spike MS MS Spike MSD MSD Limits CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg ug/kg % RPD Rec/RPD 591-78-6 2-Hexanone ND 150 133 89 148 122 83 9 65-135/20 87-68-3 Hexachlorobutadiene ND 37.5 25.1 67* 37 20.3 55* 21* 77-131/17 98-82-8 Isopropylbenzene ND 37.5 30.9 83 37 28.8 78* 7 80-124/14 99-87-6 p-Isopropyltoluene ND 37.5 28.5 76* 37 26.2 71* 8 78-122/13 108-10-1 4-Methyl-2-pentanone ND 150 144 96 148 136 92 6 70-135/18 74-83-9 Methyl bromide ND 37.5 34.0 91 37 33.1 90 3 74-130/15 74-87-3 Methyl chloride ND 37.5 37.1 99 37 35.1 95 6 65-131/22 74-95-3 Methylene bromide ND 37.5 32.4 87 37 30.5 83 6 78-124/13 75-09-2 Methylene chloride ND 37.5 28.3 76 37 28.2 76 0 75-121/16 78-93-3 Methyl ethyl ketone ND 150 124 83 148 114 77 8 70-137/21 1634-04-4 Methyl Tert Butyl Ether ND 37.5 29.2 78 37 28.2 76 3 75-127/16 91-20-3 Naphthalene ND 37.5 27.1 72 37 24.6 67 10 67-127/19 103-65-1 n-Propylbenzene ND 37.5 28.3 76 37 26.4 71* 7 75-123/13 100-42-5 Styrene ND 37.5 30.1 80 37 28.5 77* 5 78-122/12 994-05-8 Tert-Amyl Methyl Ether ND 37.5 29.3 78 37 28.6 77 2 77-127/13 75-65-0 Tert Butyl Alcohol ND 187 159 85 185 146 79 9 61-141/32 630-20-6 1,1,1,2-Tetrachloroethane ND 37.5 32.9 88 37 31.2 84 5 78-124/13 71-55-6 1,1,1-Trichloroethane ND 37.5 31.0 83 37 30.3 82 2 79-128/15 79-34-5 1,1,2,2-Tetrachloroethane ND 37.5 28.0 75 37 26.3 71 6 70-125/14 79-00-5 1,1,2-Trichloroethane ND 37.5 30.7 82 37 29.2 79 5 74-122/13 87-61-6 1,2,3-Trichlorobenzene ND 37.5 26.3 70* 37 23.5 64* 11 75-128/18 96-18-4 1,2,3-Trichloropropane ND 37.5 35.8 96 37 33.7 91 6 74-125/15 120-82-1 1,2,4-Trichlorobenzene ND 37.5 25.9 69* 37 23.1 62* 11 77-128/16 95-63-6 1,2,4-Trimethylbenzene ND 37.5 28.9 77 37 27.0 73* 7 76-121/13 108-67-8 1,3,5-Trimethylbenzene ND 37.5 29.4 78 37 27.1 73* 8 78-123/13 127-18-4 Tetrachloroethylene ND 37.5 50.4 135* 37 47.4 128* 6 77-125/14 108-88-3 Toluene ND 37.5 31.2 83 37 29.8 81 5 78-120/13 79-01-6 Trichloroethylene ND 37.5 32.6 87 37 31.4 85 4 80-124/13 75-69-4 Trichlorofluoromethane ND 37.5 35.8 96 37 33.8 91 6 78-130/17 75-01-4 Vinyl chloride ND 37.5 41.0 109 37 39.6 107 3 69-136/18 1330-20-7 Xylene (total) ND 112 92.9 83 111 88.1 79 5 78-122/13 CAS No. Surrogate Recoveries MS MSD C41974-1 Limits 1868-53-7 Dibromofluoromethane 92% 92% 92% 75-125% * = Outside of Control Limits. ■ 25 of 40 ■Accu-rEE;-r> C41950