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1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />McCampbell Analytical, Inc. <br />Web, wa mccampbeltcom E-mail: main@mccampbell.coin <br />"When Oualitv Counts" Tele hone: 877-252-9262 Fax: 925-252.9269 <br />Philip Environmental Services <br />� 535 Getty Court, Suite H <br />Benicia, CA 94510 <br />Client Project ID: LODI CHROME <br />Date Sampled: 09/07/07 <br />Date Received: 09/07/07 <br />Client Contact: TerryMcGuinness <br />Date Extracted: 09/07/07 <br />Client P.O.: 490408 <br />Date Analyzed: 09/11/07-09/14/07 <br />CAM / CCR 17 Metals* <br />Lab ID <br />0709126-OOIA <br />0709126-002A <br />0709126-003A <br />0709126-004A <br />Reporting Limit for DF =1; <br />ND means not detectcd <br />above the reporting limit <br />Client ID <br />FR I <br />FR 2 <br />FR 3 <br />FR 4 <br />Matrix <br />W <br />W <br />W <br />W <br />s W <br />Extraction Type <br />TOTAL <br />TOTAL <br />TOTAI, <br />TOTAL, <br />mg,kg µg L <br />ICP -MS Metals, Concentration* <br />Analvocal Method: E200,8 Extraoon Method. E200,8 <br />d 709 <br />Dilution Factor 20 20 20 <br />1 1 1 <br />Antimonv 23 ND<10 ND<10 <br />6 8 NA 0.5 <br />Arsenic 28 47 17 <br />14 NA 0.5 <br />Barium 390 1100 400 <br />1900 NA 5.0 <br />Beryllium ND<10 ND<10 ND<10 <br />ND<1.0 NA 0.5 <br />Cadmium 21 120 47 <br />35 NA 025 <br />Chromium 560 3000 780 <br />3100 NA 0.5 <br />Cobalt 110 540 82 <br />69 NA 0.5 <br />Copper 28,000 29,000 8900 <br />5900 NA 0.5 <br />Lead 1600 690 660 <br />620 NA 0.5 <br />Mercury 6.8 1 4 2.4 <br />0 82 NA 0.012 <br />Molybdenum 1 42 33 <br />Nickel 20,000280,000 44-000 <br />25 0 NA 0 5 <br />Selenium 2 13 <br />13 NA 5 <br />Silver 21 31 2R <br />7.4 NA 0. <br />Thallium ND<10 ND<10 ND<10 <br />Vanadium 62 370 78 <br />ND NA 0 <br />110 0.5 <br />Zinc 19 000 00 9500 <br />6400 NA 5. <br />%SS 26 98 98 <br />92 <br />Comments k k k <br />k <br />*water samples are reported in µg/L, product/oil/non-aqueous liquid samples and all TCLP ! STLC / DISTLC % SPLP extracts are reported in <br />mg/L, soil/sludge/solid samples in mg/kg, wipe samples in pg/wipe, filter samples in µg/filter. <br />9 means surrogate diluted out of range; ND means not detected above the reporting limit', N/A means not applicable to this sample or <br />instrument. <br />TOTAL = acid digestion. <br />WET = Waste Extraction Test (STLC). <br />DI WET = Waste Extraction Test using de -ionized water. <br />i) aqueous sample containing greater than —1 vol. % sediment, for DISSOLVED metals, this sample has been preserved prior to filtration; for <br />TOTAL^ metals, a representative sediment -water mixture was digested; j) reporting limit raised due to insufficient sample amount; .1) analyte <br />detected below quantitation limits; k) reporting limit raised due to matrix interfcrencc; m) estimated value due to low/high surrrogate recovery, <br />caused by matrix interference; n) results are reported on a dry weight basis; p see attached narrative. <br />DHS ELAP Certification No 1644 Angela Rydelius, Lab Manager <br />