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McCampbell Analytical* Inc. <br />ad, <br />1534 Willow Pass RoPittsburg, CA 94565-1701 <br />e f-, <br />Web: www.mccampbell.com E-mail: mairi@mccarnpbell.com <br />"When Ouality Counts" <br />Telephone: 877-252-9262 Fax: 925-252-9269 <br />Philip Environmental Services <br />Client Project ID: LODI CHROME <br />Date Sampled: <br />09/07/07 <br />Date Received: <br />09/07/07 <br />535 Getty Court, Suite H <br />Client Contact: Tent' McGuinness <br />Date Extracted: <br />09/07/07 <br />Benicia, CA 94510 <br />Client P.O.: #90408 <br />Date Analyzed: <br />09/11/07-09/14/07 <br />CAM / CCR 17 Metals* <br />Lab ID 0709126-005A 0709126-006A 0709126-007A <br />0709126-008A <br />FR 8 <br />Reporting Limit for DF =1; <br />ND means not detected <br />Client ID <br />FR 5 <br />FR 6 <br />FR 7 <br />above the reporting limit <br />Matrix <br />W <br />W <br />W W <br />s IN <br />Extraction Type TOTAL TOTAL TOTAL TOTAL <br />mg/kg lig/l, <br />ICP -MS Metals, Concentration* <br />L_nalvticalMctho& <br />E200.8 Extraction thod: E200.8 <br />Work Or, 0709126 <br />Dilution Factor I 1 I 1 <br />1 i <br />Antimony 2.8 5.0 2.5 11 <br />NA 0.5 <br />Arsenic 16 15 18 14 <br />NA 0.5 <br />Barium 480 450 1100 260 <br />NA 5.0 <br />Beryllium ND<1.0 ND<1.0 ND<1.0 ND<1.0 <br />NA 0.5 <br />Cadmium 45 23 77 23 <br />NA 0.25 <br />Chromium 800 670 530 440 <br />NA 0.5 <br />Cobalt 36 77 37 38 <br />NA 0.5 <br />Copper 4200 13.000 5500 12,000 <br />NA 0.5 <br />Lead 310 660 200 710 <br />NA 0.5 <br />Mercury 1.1 1.7 1.4 2.1 <br />NA 0.012 <br />Mol bden m 23 8.3 92 14 <br />NA 0.5 <br />Nickel 13,0000 5800 9200 <br />NA 0.5 <br />Selenium 2.7 2.7 4.5 2.4 <br />NA 0.5 <br />Silver 16 13 8.4 18 <br />N A 0.19 <br />Thallium D ND ND ND <br />NA 0. <br />Vanadium 80 74 100 48 <br />NA 0 <br />Zinc 6000 9300 4900 11,000 <br />NA 5.0 <br />0/0S& 10 <br />Comments k k k k <br />*water samples are reported in µg/L, product/oil/non-aqueous liquid samples and all TCLP / STLC / DISTLC / SPLP extracts are reported in <br />mg/L, soil/sludge/solid samples in mg/kg, wipe samples in µg/wipe, filter samples in µg/filter. <br /># means surrogate diluted out of range; ND means not detected above the reporting limit; N/A means not applicable to this sample or <br />instrument. <br />TOTAL = acid digestion. <br />WET = Waste Extraction Test (STLC). <br />DI WET = Waste Extraction Test using de -ionized water. <br />i) aqueous sample containing greater than -1 vol. % sediment; for DISSOLVED metals, this sample has been preserved <br />prior to filtration; for <br />TOTAL^ metals, a representative sediment -water mixture was digested; j) reporting limit raised due to insufficient sample amount, J) analyte <br />detected below quantitation limits; k) reporting limit raised due to matrix interference; m) estimated value due to low/high <br />surrrogate recovery, <br />caused by matrix interference; n) results are reported on a dry weight basis; ) see attached narrative. <br />DHS ELAP Certification No 1644 � Angela Rydelius, Lab Manager <br />