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WG1561589 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. <br /> Volatile Organic Compounds (GC/MS) by Method 82608 L1273022-01 <br /> Laboratory Control Sample(LCS) <br /> (LCS)R3583233-1 10/19/2010:28 C( <br /> Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier <br /> Analyte mg/kg mg/kg % % E <br /> Naphthalene 0.125 0.0942 75.4 59.0-130 <br /> n-Propylbenzene 0.125 0.135 108 74.0-126 EStyrene 0.125 0.128 102 72.0-127 <br /> 1,1,1,2-Tetrachloroethane 0.125 0.137 110 74.0-129 <br /> 1,1,2,2-Tetrachloroethane 0.125 0.127 102 68.0-128 Rn <br /> Tetrachloroethene 0.125 0.131 105 70.0-136 <br /> Toluene 0.125 0.134 107 75.0421 <br /> 1,1,2-Trichlorotrifluoroethane 0.125 0.119 95.2 61.0-139 qr <br /> 1,2,3-Trichlorobenzene 0.125 0.0922 73.8 59.0-139 <br /> 1,2,4-Trichlorobenzene 0.125 0.122 97.6 62.0-137 <br /> 1,1,1-Trichloroethane 0.125 0.151 121 69.0-126 <br /> 1,1,2-Trichloroethane 0.125 0.136 109 78.0-123 GI <br /> Trichloroethene 0.125 0.139 111 76.0-126 <br /> Trichlorofluoromethane 0.125 0.140 112 61.0-142 <br /> 1,2,3-Trichloropropane 0.125 0.142 114 67.0-129 ^AI <br /> 1,2,3-Trimethylbenzene 0.125 0.125 100 74.0-124 <br /> 1,2,4-Trimethylbenzene 0.125 0.129 103 70.0-126 <br /> 1,3,5-Trimethylbenzene 0.125 0.134 107 73.0-127 17C <br /> Vinyl chloride 0.125 0.114 91.2 63.0-134 <br /> Xylenes,Total 0.375 0.390 104 72.0-127 <br /> (S)Toluene-d8 97.6 75.0-131 <br /> (S)4-Bromofluorobenzene 98.4 67.0-138 <br /> (S)1,2-Dichloroethone-d4 102 70.0-130 <br /> L1272707-09 Original Sample(OS) • Matrix Spike (MS) • Matrix Spike Duplicate(MSD) <br /> (OS)L1272707-09 10/19/2016:51•(MS)R3583233-3 10/19/2019:04.(MSD)R3583233-4 10/19/2019:23 <br /> Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits <br /> Analyte mg/kg mg/kg mg/kg mg/kg % % % % % <br /> Acetone 0.559 U 0.190 0.184 42.7 41.3 1 10.0-160 3.21 40 <br /> Acrylonitrile 0.559 U 0.452 0.377 102 84.7 1 10.0-160 18.1 40 <br /> Benzene 0.112 U 0.0635 0.0420 71.3 47.2 1 10.0-149 J3 40.8 37 <br /> Bromobenzene 0.112 U 0.0734 0.0544 82.5 61.1 1 10.0-156 29.7 38 <br /> Bromodichloromethane 0.112 U 0.0738 0.0559 82.9 62.8 1 10.0-143 27.6 37 <br /> Bromoform 0.112 U 0.0927 0.0778 104 87.4 1 10.0-146 17.5 36 <br /> Bromomethane 0.112 U 0.0362 0.0240 40.7 27.0 1 10.0-149 J3 40.5 38 <br /> n-Butylbenzene 0.112 U 0.0626 0.0370 70.3 41.6 1 10.0-160 J3 51.4 40 <br /> sec-Butylbenzene 0.112 U 0.0619 0.0361 69.6 40.6 1 10.0-159 J3 52.7 39 <br /> tert-Butylbenzene 0.112 U 0.0615 0.0373 69.1 41.9 1 10.0-156 J3 49.0 39 <br /> ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: <br /> UPRR-Patriot Environmental Services 11-20-00448 L1273022 10/22/2011:43 16 of 23 <br />