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WG1561589 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 82608 L1273022-01 L1272707-09 Original Sample(OS) • Matrix Spike(MS) • Matrix Spike Duplicate(MSD) (OS)L1272707-09 10/19/2016:51•(MS)R3583233-3 10/19/2019:04•(MSD)R3583233-4 10/19/2019:23 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg % % % % % Tri Carbon tetrachloride 0.112 U 0.0412 0.0277 46.3 31.1 1 10.0-145 J3 39.2 37 Chlorobenzene 0.112 U 0.0646 0.0460 72.6 51.7 1 10.0-152 33.6 39 SS Chlorodibromomethane 0.112 U 0.0840 0.0680 94.4 76.4 1 10.0-146 21.1 37 Chloroethane 0.112 U 0.0311 0.0170 34.9 19.1 1 10.0446 J3 58.6 40 Fn ]Chloroform 0.112 U 0.0725 0.0494 81.5 55.5 1 10.0-146 J3 37.9 37 fl Chloromethane 0.112 U 0.0493 0.0283 55.4 31.8 1 10.0459 J3 54.1 37 2-Chlorotoluene 0.112 U 0.0649 0.0437 72.9 49.1 1 10.0459 J3 39.0 38 Fr 4-Chlorotoluene 0.112 U 0.0647 0.0473 72.7 53.1 1 10.0-155 31.1 39 1,2-Dibromo-3-Chloropropane 0.112 U 0.0640 0.0637 71.9 71.6 1 10.0-151 0.470 39 1,2-Dibromoethane 0.112 U 0.0911 0.0768 102 86.3 1 10.0-148 17.0 34 Dibromomethane 0.112 U 0.0913 0.0731 103 82.1 1 10.0-147 22.1 35 1,2-Dichlorobenzene 0.112 U 0.0761 0.0578 85.5 64.9 1 10.0-155 27.3 37 7G1 1,3-Dichlorobenzene 0.112 U 0.0719 0.0515 80.8 57.9 1 10.0-153 33.1 38 1,4-Dichlorobenzene 0.112 U 0.0713 0.0549 80.1 61.7 1 10.0-151 26.0 38 Dichlorodifluoromethane 0.112 U 0.0487 0.0258 54.7 29.0 1 10.0-160 J3 61.5 35 FAI 1,1-Dichioroethane 0.112 U 0.0665 0.0418 74.7 47.0 1 10.0-147 J3 45.6 37 1,2-Dichioroethane 0.112 U 0.0801 0.0669 90.0 75.2 1 10.0-148 18.0 35 FS 1,1-Dichloroethene 0.112 U 0.0518 0.0292 58.2 32.8 1 10.0-155 J3 55.8 37 cis-1,2-Dichloroethene 0.112 U 0.0652 0.0449 73.3 50.4 1 10.0-149 36.9 37 trans-1,2-Dichloroethene 0.112 U 0.0607 0.0341 68.2 38.3 1 10.0-150 J3 56.1 37 1,2-Dichloropropane 0.112 U 0.0714 0.0527 80.2 59.2 1 10.0-148 30.1 37 1,1-Dichloropropene 0.112 U 0.0497 0.0277 55.8 31.1 1 10.0-153 J3 56.8 35 1,3-Dichloropropane 0.112 U 0.0826 0.0679 92.8 76.3 1 10.0-154 19.5 35 cis-1,3-Dichloropropene 0.112 U 0.0771 0.0564 86.6 63.4 1 10.0-151 31.0 37 trans-1,3-Dichloropropene 0.112 U 0.0805 0.0646 90.4 72.6 1 10.0-148 21.9 37 2,2-Dichloropropane 0.112 U 0.0467 0.0262 52.5 29.4 1 10.0-138 J3 56.2 36 Di-isopropyl ether 0.112 U 0.0818 0.0611 91.9 68.7 1 10.0-147 29.0 36 Ethylbenzene 0.112 U 0.0593 0.0383 66.6 43.0 1 10.0-160 J3 43.0 38 Hexachloro-1,3-butadiene 0.112 U 0.0653 0.0416 73.4 46.7 1 10.0-160 J3 44.3 40 Isopropylbenzene 0.112 U 0.0621 0.0373 69.8 41.9 1 10.0-155 J3 49.9 38 p-Isopropyltoluene 0.112 U 0.0642 0.0394 72.1 44.3 1 10.0-160 J3 47.9 40 2-Butanone(MEK) 0.559 U 0.373 0.432 83.8 97.1 1 10.0-160 14.7 40 Methylene Chloride 0.112 U 0.0679 0.0509 76.3 57.2 1 10.0-141 28.6 37 4-Methyl-2-pentanone(MIBK) 0.559 U 0.443 0.413 99.6 92.8 1 10.0-160 7.01 35 Methyl tert-butyl ether 0.112 U 0.0793 0.0703 89.1 79.0 1 11.0447 12.0 35 Naphthalene 0.112 U 0.0635 0.0665 71.3 74.7 1 10.0-160 4.62 36 n-Propylbenzene 0.112 U 0.0604 0.0367 67.9 41.2 1 10.0-158 J3 48.8 38 Styrene 0.112 U 0.0664 0.0473 74.6 53.1 1 10.0460 33.6 40 1,1,1,2-Tetrachloroethane 0.112 U 0.0755 0.0569 84.8 63.9 1 10.0-149 28.1 39 1,1,2,2-Tetrachloroethane 0.112 U 0.0825 0.0769 92.7 86.4 1 10.0-160 7.03 35 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-Patriot Environmental Services 11-20-00448 L1273022 10/22/2011:43 17 of 23