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WG1561589 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 82608 L1273022-01 L1272707-09 Original Sample(OS) • Matrix Spike(MS) • Matrix Spike Duplicate(MSD) (OS)L1272707-09 10/19/2016:51•(MS)R3583233-3 10/19/2019:04•(MSD)R3583233-4 10/19/2019:23 Rp Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits Anatyte mg/kg mg/kg mg/kg mg/kg % % % % % TC --------- --------- --------------- Tetrachloroethene 0.112 U 0.0541 0.0310 60.8 34.8 1 10.0-156 J3 54.3 39 Toluene 0.112 U 0.0632 0.0405 71.0 45.5 1 10.0-156 J3 43.8 38 SS 1,1,2-Trichlorotrifluoroethane 0.112 U 0.0403 0.0216 45.3 24.3 1 10.0-160 J3 60.4 36 1,2,3-Trichlorobenzene 0.112 U 0.0640 0.0641 71.9 72.0 1 10.0-160 0.156 40 Rn 1,2,4-Trichlorobenzene 0.112 U 0.0757 0.0661 85.1 74.3 1 10.0-160 13.5 40 1,1,1-Trichloroethane 0.112 U 0.0527 0.0299 59.2 33.6 1 10.0-144 J3 55.2 35 1,1,2-Trichloroethane 0.112 U 0.0917 0.0754 103 84.7 1 10.0-160 19.5 35 S r Trichloroethene 0.112 0.00243 0.0618 0.0381 66.7 40.1 1 10.0-156 J3 47.4 38 Trichlorofluoromethane 0.112 U 0.0359 0.0184 40.3 20.7 1 10.0-160 J3 64.5 40 1,2,3-Tdchloropropane 0.112 U 0.0940 0.0841 106 94.5 1 10.0-156 11.1 35 1,2,3-Trimethylbenzene 0.112 U 0.0679 0.0492 76.3 55.3 1 10.0-160 31.9 36 1,2,4-Trimethylbenzene 0.112 U 0.0634 0.0425 71.2 47.8 1 10.0-160 J3 39.5 36 G I 1,3,5-Trimethyibenzene 0.112 U 0.0644 0.0415 72.4 46.6 1 10.0-160 J3 43.2 38 Vinyl chloride 0.112 U 0.0450 0.0217 50.6 24.4 1 10.0-160 J3 69.9 37 Xylenes,Total 0.336 U 0.187 0.115 70.0 43.1 1 10.0-160 J3 47.7 38 AI (S)Toluene-d8 101 99.6 75.0-131 (S)4-Bromofluorobenzene 98.2 974 67.0-138 FC ](S)1,2-Dichloroethone-d4 104 104 70.0-130 C ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-Patriot Environmental Services 11-20-00448 L1273022 10/22/2011:43 18 of 23