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SAMPLE #1 SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. Collected date/time: 02109/20 13:00 L1191356 Volatile Organic Compounds (GC/MS) by Method 82608 Result Qualifier MDL RDL Dilution Analysis Batch RP Analyte mg/kg mg/kg mg/kg date/time 1,2-Dibromo-3-Chloropropane U 0.0103 0.0503 2.01 02/23/202012:05 WG1432694 zTC 1,2-Dibromoethane U 0.00106 0.00503 2.01 02/23/202012:05 WG1432694 Dibromomethane U 0.00201 0.0101 2.01 02/23/202012:05 WG1432694 FS 1,2-Dichlorobenzene U 0.00291 0.0101 2.01 02/23/202012:05 WG1432694 1,3-Dichlorobenzene U 0.00342 0.0101 2.01 02/23/2020 12:05 WG1432694 1,4-Dichlorobenzene U 0.00396 0.0101 2.01 02/23/2020 12:05 WG1432694 Rn Dichlorodifluoromethane U 0.00164 0.00503 2.01 02/23/202012:05 WG1432694 1,1-Dichloroethane U 0.00116 0.00503 2.01 02/23/202012:05 WG1432694 1,2-Dichloroethane U 0.000955 0.00503 2.01 02/23/202012:05 WG1432694 1,1-Dichloroethene U 0.00101 0.00503 2.01 02/23/202012:05 WG1432694 cis-1,2-Dichloroethene U 0.00139 0.00503 2.01 02/23/202012:05 WG1432694 "OC trans-1,2-Dichloroethene U 0.00287 0.0101 2.01 02/23/202012:05 WG1432694 1,2-Dichloropropane U 0.00255 0.0101 2.01 02/23/202012:05 WG1432694 1,1-Dichloropropene U J4 0.00141 0.00503 2.01 02/23/202012:05 WG1432694 GI 1,3-Dichloropropane U 0.00352 0.0101 2.01 02/23/202012:05 WG1432694 cis-1,3-Dichloropropene U 0.00136 0.00503 2.01 02/23/202012:05 WG1432694 AI trans-1,3-Dichloropropene U 0.00308 0.0101 2.01 02/23/202012:05 WG1432694 2,2-Dichloropropane U 0.00159 0.00503 2.01 02/23/202012:05 WG1432694 Di-isopropyl ether U 0.000704 0.00201 2.01 02/23/202012:05 WG1432694 SC Ethylbenzene U 0.00107 0.00503 2.01 02/23/202012:05 WG1432694 Hexachloro-1,3-butadiene U J3 0.0255 0.0503 2.01 02/23/202012:05 WG1432694 Isopropylbenzene U 0.00173 0.00503 2.01 02/23/202012:05 WG1432694 p-Isopropyltoluene 0.00709 J 0.00468 0.0101 2.01 02/23/202012:05 WG1432694 2-Butanone(MEK) 0.104 B 0.0251 0.0503 2.01 02/23/202012:05 WG1432694 Methylene Chloride U 0.0133 0.0503 2.01 02/23/202012:05 WG1432694 4-Methyl-2-pentanone(MIBK) U 0.0201 0.0503 1.01 02/23/202012:05 WG1432694 Methyl tert-butyl ether U 0.000593 0.00201 2.01 02123/202012:05 WG1432694 Naphthalene 0.0135 1 0.00627 0.0251 2.01 02/23/202012:05 WG1432694 n-Propylbenzene 0.00583 J 0.00237 0.0101 2.01 02/23/202012:05 WG1432694 Styrene U 0.00549 0.0251 2.01 02/23/202012:05 WG1432694 1,1,1,2-Tetrachloroethane U 0.00101 0.00503 2.01 02/23/202012:05 WG1432694 1,1,2,2-Tetrachloroethane U 0.000784 0.00503 2.01 02/23/202012:05 WG1432694 1,1,2-Trichlorotrifluoroethane U 0.00136 0.00503 2.01 02/23/202012:05 WG1432694 Tetrachloroethene U 0.00141 0.00503 2.01 02/23/202012:05 WG1432694 Toluene 0.00523 J 0.00251 0.0101 2.01 02/23/202012:05 WG1432694 1,2,3-Trichlorobenzene U J3 0.00126 0.0251 2.01 02/23/202012:05 WG1432694 1,2,4-Trichlorobenzene U 0.00969 0.0251 2.01 02/23/202012:05 WG1432694 1,1,1-Trichloroethane U 0.000553 0.00503 2.01 02/23/202012:05 WG1432694 1,1,2-Trichloroethane U 0.00177 0.00503 2.01 02/23/202012:05 WG1432694 Trichloroethene U 0.000804 0.00201 2.01 02/23/202012:05 WG1432694 Trichlorofluoromethane U 0.00101 0.00503 2.01 02/23/202012:05 WG1432694 1,2,3-Trichloropropane U 0.0103 0.0251 2.01 02/23/202012:05 WG1432694 1,2,4-Trimethylbenzene 0.0553 0.00233 0.0101 2.01 02/23/202012:05 WG1432694 1,2,3-Trimethylbenzene 0.0219 0.00231 0.0101 2.01 02/23/202012:05 WG1432694 1,3,5-Trimethylbenzene 0.0148 0.00217 0.0101 2.01 02/23/202012:05 WG1432694 Vinyl chloride U 0.00137 0.00503 2.01 02/23/202012:05 WG1432694 Xylenes,Total 0.0243 0.00961 0.0131 2.01 02/23/2020 12:05 WG1432694 (S)Toluene-d8 107 75.0-131 021231202012.05 WG1432694 (S)4-Bromofluorobenzene 102 67.0-138 02/23/202012:05 WG1432694 (S)1,2-Dichloroethone-0 89.1 70.0-130 021231202012.05 WG1432694 ACCOUNT: PROJECT: SDG: DATElrIM E: PAGE: UPRR-Patriot Environmental Services 11-20-00061 L1191356 02/25/2014:54 6 of 27