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SAMPLE #1 SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. Collected date/time: 02/09/20 13:00 L1191356 Semi-Volatile Organic Compounds (GC) by Method 8015 Result Qualifier MDL RDL Dilution Analysis Batch CP] Analyte mg/kg mg/kg rng/kg date/time C12-C22 Hydrocarbons 68.5 2.20 12.0 3 - 02/24/2020 04:55 WG1432019 FTC C22-02 Hydrocarbons 18.7 3.99 12.0 3 02/24/2020 04:55 WG1432019 C32-C40 Hydrocarbons 7.89 1 3.99 12.0 3 02/24/2020 04:55 WG1432019 (S)c-Terphenyl 61.0 18.0-148 0212412020 04:55 WG1432019 Rs Sample Narrative: Fn] L1191356-01 WG1432019:Dilution due to matrix impact during extraction procedure Semi Volatile Organic Compounds (GC/MS) by Method 827OC Result Qualifier MDL RDL Dilution Analysis Batch e Analyte mg/kg mg/kg mg/kg date/time Qc Acenaphthene U 0.0193 0.0999 3 02/23/202013:29 WG1432236 Acenaphthylene U 0.0201 0.0999 3 02/23/202013:29 WG1432236 FGI Anthracene U 0.0190 0.0999 3 02/23/202013:29 WG1432236 Benzidine U 0.191 0.999 3 02/23/202013:29 WG1432236 Benzo(a)anthracene U 0.0128 0.0999 3 02/23/202013:29 WG1432236 A Benzo(b)fluoranthene U 0.0209 0.0999 3 02/23/202013:29 WG1432236 Benzo(k)fluoranthene U 0.0175 0.0999 3 02/23/202013:29 WG1432236 FCBenzo(g,h,i)perylene U 0.0216 0.0999 3 02/23/202013:29 WG1432236 Benzo(a)pyrene U 0.0164 0.0999 3 02/23/202013:29 WG1432236 Bis(2-chlorethoxy)methane U 0.0231 0.999 3 02/23/202013:29 WG1432236 Bis(2-chloroethyl)ether U 0.0269 0.999 3 02/23/202013:29 WG1432236 2,2-Oxybis(1-Chloropropane) U 0.0228 0.999 3 02/23/202013:29 WG1432236 4-Bromophenyl-phenylether U 0.0342 0.999 3 02/23/202013:29 WG1432236 2-Chloronaphthalene U 0.0192 0.0999 3 02/23/202013:29 WG1432236 4-Chlorophenyl-phenylether U 0.0188 0.999 3 02/23/202013:29 WG1432236 Chrysene U 0.0167 0.0999 3 02/23/202013:29 WG1432236 Dibenz(a,h)anthrecene U 0.0246 0.0999 3 02/23/202013:29 WG1432236 3,3-Dichlorobenzidine U 0.238 0.999 3 02/23/202013:29 WG1432236 2,4-Dinitrotoluene U 0.0182 0.999 3 02/23/202013:29 WG1432236 2,6-DinRrotoluene U 0.0221 0.999 3 02/23/202013:29 WG1432236 Fluoranthene U 0.0149 0.0999 3 02/23/202013:29 WG1432236 Fluorene U 0.0205 0.0999 3 02/23/202013:29 WG1432236 Hexachlorobenzene U 0.0257 0.999 3 02/23/202013:29 WG1432236 Hexachloro-1,3-butadiene U 0.0300 0.999 3 02/23/202013:29 WG1432236 Hexachlorocyclopentadiene U 0.176 0.999 3 02/23/202013:29 WG1432236 Hexachloroethane U 0.0402 0.999 3 02/23/202013:29 WG1432236 Indeno(1,2,3-cd)pyrene U 0.0232 0.0999 3 02/23/202013:29 WG1432236 Isophorone U 0.0157 0.999 3 02/23/202013:29 WG1432236 Naphthalene U 0.0267 0.0999 3 02/23/202013:29 WG1432236 Nitrobenzene U 0.0209 0.999 3 02/23/202013:29 WG1432236 n-Nitrosodimethylamine U 0.194 0.999 3 02/23/202013:29 WG1432236 n-Nitrosodiphenylamine U 0.270 0.999 3 02/23/202013:29 WG1432236 n-N itrosod i-n-propyla mine U 0.0272 0.999 3 02/23/202013:29 WG1432236 Phenanthrene U 0.0158 0.0999 3 02/23/202013:29 WG1432236 Benrylbutyl phthalate U 0.0309 0.999 3 02/23/202013:29 WG1432236 Bis(2-ethylhexyl)phthalate U 0.0360 0.999 3 02/23/202013:29 WG1432236 Di-n-butyl phthalate U 0.0327 0.999 3 02/23/202013:29 WG1432236 Diethyl phthalate U 0.0207 0.999 3 02/23/202013:29 WG1432236 Dimethyl phthalate U 0.0162 0.999 3 02/23/202013:29 WG1432236 Di-n-octyl phthalate U 0.0272 0.999 3 02/23/202013:29 WG1432236 Pyrene U 0.0369 0.0999 3 02/23/202013:29 WG1432236 Pyridine U 0.188 0.999 3 02/23/202013:29 WG1432236 1,2,4-Trichlorobenzene U 0.0263 0.999 3 02/23/202013:29 WG1432236 4-Chloro-3-methylphenol U 0.0143 0.999 3 02/23/202013:29 WG1432236 2-Chlorophenol U 0.0249 0.999 3 02/23/202013:29 WG1432236 ACCOUNT: PROJECT. SDG: DATE/TIME: PAGE: UPRR-Patriot Environmental Services 11-20-00061 L1191356 02/25/2014:54 7 of 27