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WG1432694 QUALITY CONTROL SUMMARY ONE LAB,NATIONWIDE. <br /> Volatile Organic Compounds (GC/MS) by Method 8260B L1191356-01 <br /> Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate(LCSD) <br /> (LCS)R3502473-1 02/23/20 09:47•(LCSD)R3502473-2 02/23/2010:07 Fr) <br /> Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits <br /> Analyte mg/kg mg/kg mg/kg % % % % % TC <br /> ----------- <br /> Naphthalene <br /> ------Naphthalene 0.125 0.109 0.115 87.2 92.0 59.0-130 5.36 20 <br /> n-Propylbenzene 0.125 0.114 0.125 91.2 100 74.0-126 9.21 20 3 <br /> Ss <br /> Styrene 0.125 0.114 0.117 91.2 93.6 72.0-127 2.60 20 <br /> 1,1,1,2-Tetrachloroethane 0.125 0.112 0.111 89.6 88.8 74.0-129 0.897 20 Fn 1,1,2,2-Tetrachloroethane 0.125 0.123 0.119 98.4 95.2 68.0-128 3.31 20 <br /> Tetrachloroethene 0.125 0.126 0.134 101 107 70.0-136 6.15 20 <br /> Toluene 0.125 0.118 0.123 94.4 98.4 75.0-121 4.15 20 SSr <br /> 1,1,2-Trichlorotrifluoroethane 0.125 0.136 0.144 109 115 61.0-139 5.71 20 <br /> 1,2,3-Tdchlorobenzene 0.125 0.0761 0.0954 60.9 76.3 59.0-139 J3 22.5 20 <br /> 1,2,4-Trichlorobenzene 0.125 0.123 0.138 98.4 110 62.0-137 11.5 20 <br /> 1,1,1-Trichloroethane 0.125 0.106 0.110 84.8 88.0 69.0-126 3.70 20 <br /> 1,1,2-Trichloroethane 0.125 0.130 0.134 104 107 78.0-123 3.03 20 'GI <br /> Trichloroethene 0.125 0.131 0.129 105 103 76.0-126 1.54 20 <br /> Trichlorofluoromethane 0.125 0.118 0.117 94.4 93.6 61.0-142 0.851 20 <br /> 1,2,3-Trichloropropane 0.125 0.114 0.118 91.2 94.4 67.0-129 3.45 20 AI <br /> 1,2,3-Trimethylbenzene 0.125 0.0961 0.0974 76.9 77.9 74.0-124 1.34 20 <br /> 1,2,4-Trimethylbenzene 0.125 0.103 0.108 82.4 86.4 70.0-126 4.74 20 e <br /> Sc <br /> 1,3,5-Trimethylbenzene 0.125 0.121 0.126 96.8 101 73.0-127 4.05 20 <br /> Vinyl chloride 0.125 0.113 0.117 90.4 93.6 63.0-134 3.48 20 <br /> Xylenes,Total 0.375 0.349 0.364 93.1 97.1 72.0-127 4.21 20 <br /> (S)Toluene-d8 103 103 75.0-131 <br /> (S)4-Bromolluorobenzene 101 104 67.0-138 <br /> (S)1,2-Dichloroethane-d4 99.6 96.9 70.0-130 <br /> L1191346-08 Original Sample (OS) • Matrix Spike(MS) • Matrix Spike Duplicate(MSD) <br /> (OS)L1191346-08 02/23/20 17:33•(MS)R3502473-4 02/23/2018:13•(MSD)R3502473-5 02/23/2018:32 <br /> Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits <br /> Analyte mg/kg mg/kg mg/kg mg/kg % % % % % <br /> Acetone 0.625 ND 0.113 0.908 18.1 145 1 10.0-160 J3 156 40 <br /> Acrylonitrile 0.625 ND 0.303 0.169 48.5 27.0 1 10.0-160 J3 56.8 40 <br /> Benzene 0.125 ND 0.115 0.114 92.0 91.2 1 10.0-149 0.873 37 <br /> Bromobenzene 0.125 ND 0.134 0.130 107 104 1 10.0-156 3.03 38 <br /> Bromodichloromethane 0.125 ND 0.112 0.112 89.6 89.6 1 10.0-143 0.000 37 <br /> Bromoform 0.125 ND 0.0949 0.0854 75.9 68.3 1 10.0-146 10.5 36 <br /> Bromomethane 0.125 ND 0.103 0.107 82.4 85.6 1 10.0-149 3.81 38 <br /> n-Butylbenzene 0.125 ND 0.209 0.211 167 169 1 10.0-160 J5 J5 0.952 40 <br /> sec-Butylbenzene 0.125 ND 0.165 0.181 132 145 1 10.0-159 9.25 39 <br /> tert-Butylbenzene 0.125 ND 0.196 0.210 157 168 1 10.0-156 J5 J5 6.90 39 <br /> ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: <br /> UPRR-Patriot Environmental Services 11-20-00061 L1191356 02/25/2014:54 17 of 27 <br />