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WG1432694 QUALITY CONTROL SUMMARY ONE LAB.NATIONVADE. Volatile Organic Compounds (GC/MS) by Method 82608 L1191356-01 L1191346-08 Original Sample(OS) • Matrix Spike(MS) • Matrix Spike Duplicate(MSD) ❑ (CGS)L1191346-08 02/23/2017:33•(MS)R3502473-4 02/23/2018:13•(MSD)R3502473-5 02/23/2018:32 Cp Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Oualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg % % % % % TC Carbon tetrachloride 0.125 ND 0.107 0.107 85.6 85.6 1 10.0-145 0.000 37 Chlorobenzene 0.125 ND 0.126 0.124 101 99.2 1 10.0-152 1.60 39 SS Chlorodibromomethane 0.125 ND 0.118 0.106 94.4 84.8 1 10.0-146 10.7 37 Chloroethane 0.125 NO 0.123 0.136 98.4 109 1 10.0-146 10.0 40 Rn Chloroform 0.125 ND 0.103 0.108 82.4 86.4 1 10.0-146 4.74 37 Chloromethane 0.125 ND 0.139 0.139 111 111 1 10.0-159 0.000 37 2-Chlorotoluene 0.125 ND 0.155 0.162 124 130 1 10.0-159 4.42 38 Fr] 4-Chlorotoluene 0.125 ND 0.163 0.171 130 137 1 10.0-155 4.79 39 1,2-Dibromo-3-Chloropropane 0.125 ND 0.0852 0.0636 68.2 50.9 1 10.0-151 29.0 39 1,2-Dibromoethane 0.125 ND 0.120 0.106 96.0 84.8 1 10.0-148 12.4 34 Dibromomethane 0.125 ND 0.0780 0.0712 62.4 57.0 1 10.0-147 9.12 35 1,2-Dichlorobenzene 0.125 ND 0.131 0.138 105 110 1 10.0-155 5.20 37 GI 1,3-Dichlorobenzene 0.125 ND 0.131 0.141 105 113 1 10.0-153 7.35 38 1,4-Dichlorobenzene 0.125 ND 0.131 0.134 105 107 1 10.0-151 2.26 38 Dichlorodifluoromethane 0.125 ND 0.170 0.192 136 154 1 10.0-160 12.2 35 [7] 1,1-Dichloroethane 0.125 ND 0.113 0.110 90.4 88.0 1 10.0-147 2.69 37 1,2-Dichloroethane 0.125 ND 0.100 0.0837 80.0 67.0 1 10.0-148 17.7 35 FC 1,1-Dichloroethene 0.125 ND 0.131 0.142 105 114 1 10.0-155 8.06 37 cis-1,2-Dichloroethene 0.125 0.0140 0.117 0.119 82.4 84.0 1 10.0-149 1.69 37 trans-1,2-Dichloroethene 0.125 ND 0.111 0.111 88.8 88.8 1 10.0-150 0.000 37 1,2-Dichloropropane 0.125 ND 0.123 0.120 98.4 96.0 1 10.0-148 2.47 37 1,1-Dichloropropene 0.125 ND 0.108 0.111 86.4 88.8 1 10.0-153 2.74 35 1,3-Dichloropropane 0.125 ND 0.159 0.140 127 112 1 10.0-154 12.7 35 cis-1,3-Dichloropropene 0.125 ND 0.112 0.109 89.6 87.2 1 10.0451 2.71 37 trans-1,3-Dichloropropene 0.125 ND 0.116 0.105 92.8 84.0 1 10.0-148 9.95 37 2,2-Dichloropropane 0.125 ND 0.0586 0.0615 46.9 49.2 1 10.0-138 4.83 36 Di-isopropyl ether 0.125 ND 0.106 0.108 84.8 86.4 1 10.0-147 1.87 36 Ethylbenzene 0.125 ND 0.138 0.134 110 107 1 10.0460 2.94 38 Hexachloro-1,3-butadiene 0.125 ND 0.302 0.296 242 237 1 10.0-160 J5 J5 2.01 40 Isopropylbenzene 0.125 ND 0.126 0.131 101 105 1 10.0-155 3.89 38 p-Isopropyltoluene 0.125 ND 0.158 0.166 126 133 1 10.0-160 4.94 40 2-Butanone(MEK) 0.625 0.0485 0.275 0.149 36.2 16.1 1 10.0-160 J3 59.4 40 Methylene Chloride 0.125 ND 0.116 0.115 92.8 92.0 1 10.0-141 0.866 37 4-Methyl-2-pentanone(MIBK) 0.625 ND 0.558 0.379 89.3 60.6 1 10.0-160 J3 38.2 35 Methyl tent-butyl ether 0.125 ND 0.0865 0.0736 69.2 58.9 1 11.0-147 16.1 35 Naphthalene 0.125 ND 0.113 0.101 90.4 80.8 1 10.0460 11.2 36 n-Propylbenzene 0.125 ND 0.157 0.165 126 132 1 10.0458 4.97 38 Styrene 0.125 ND 0.127 0.122 102 97.6 1 10.0460 4.02 40 1,1,1,2-Tetrachloroethane 0.125 ND 0.107 0.0985 85.6 78.8 1 10.0-149 8.27 39 1,1,2,2-Tetrachloroethane 0.125 ND 0.0999 0.0852 79.9 68.2 1 10.0460 15.9 35 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-Patriot Environmental Services 11-20-00061 L1191356 02/25/2014:54 18 of 27