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WG1432694 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. <br /> Volatile Organic Compounds (GC/MS) by Method 82608 L1191356-01 <br /> L1191346-08 Original Sample(OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) --- <br /> (OS)L1191346-08 02/23/20 17:33•(MS)R3502473-4 02/23/20 18:13•(MSD)R3502473-5 02/23/20 18:32 <br /> Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits <br /> Analyte mg/kg mg/kg mg/kg mg/kg % % % % % TC <br /> Tetrachloroethene 0.125 ND 0.156 0.158 125 126 1 10.0-156 1.27 39 <br /> Toluene 0.125 ND 0.136 0.133 109 106 1 10.0-156 2.23 383 <br /> SS <br /> 1,1,2-Trichlorotrifluoroethane 0.125 ND 0.166 0.179 133 143 1 10.0-160 7.54 36 <br /> 1,2,3-Trichlorobenzene 0.125 ND 0.127 0.134 102 107 1 10.0-160 5.36 40 Rn 1,2,4-Trichlorobenzene 0.125 ND 0.212 0.212 170 170 1 10.0-160 J5 J5 0.000 40 <br /> 1,1,1-Trichloroethane 0.125 NO 0.102 0.109 81.6 87.2 1 10.0-144 6.64 35 <br /> 1,1,2-Trichloroethane 0.125 ND 0.136 0.122 109 97.6 1 10.0-160 10.9 35 s <br /> Sr <br /> Trichloroethene 0.125 ND 0.150 0.148 120 118 1 10.0-156 1.34 38 <br /> Trichlorofluoromethane 0.125 NO 0.0984 0.109 78.7 87.2 1 10.0-160 10.2 40 <br /> 1,2,3-Trichloropropane 0.125 ND 0.102 0.0852 81.6 68.2 1 10.0-156 17.9 35 <br /> 1,2,3-Trimethylbenzene 0.125 ND 0.118 0.123 94.4 98.4 1 10.0-160 4.15 36 <br /> 1,2,4-Trimethylbenzene 0.125 NO 0.137 0.140 110 112 1 10.0-160 2.17 36 FGI <br /> 1,3,5-Trimethylbenzene 0.125 ND 0.160 0.168 128 134 1 10.0-160 4.88 38 <br /> Vinyl chloride 0.125 ND 0.146 0.153 117 122 1 10.0-160 4.68 37 <br /> Xylenes,Total 0.375 ND 0.368 0.409 98.1 109 1 10.0-160 10.6 38 AI <br /> (S)Toluene-d8 102 102 75.0-131 <br /> (S)4-Bromof/uorobenzene 102 974 67.0-1389 <br /> SC <br /> (S)1,2-Dichloroethone-d4 75.9 76.0 70.0-130 <br /> ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: <br /> UPRR-Patriot Environmental Services 11-20-00061 L1191356 02/25/2014:54 19 of 27 <br />