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SunStar 25712 Commercentre Drive <br /> Laboratories, Inc. Lake Forest,California 92630 <br /> PROVIDING Qu AL.rrr.ANAM KICAt.Sr,Rvu r;N,n•[o!vwI[>e. 949.297.5020 Phone <br /> 949.297.5027 Fax <br /> WGR Project: NuStar Stockton Terminal <br /> 11021 Winners Circle Suite 101 Project Number: [none] Reported: <br /> Los Alamitos CA,90720 Project Manager: Gray Martz 03/17/2108:12 <br /> Volatile Organic Compounds by EPA Method 8260B-Quality Control <br /> SunStar Laboratories,Inc. <br /> Reporting Spike Source °i6REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 1031037-EPA 5030 GCMS <br /> LCS(1031037-BSI) Prepared:03/10/21 Analyzed:03/11/21 <br /> Chlorobcnzene 53.0 2.5 ug/kg 50.0 106 65.2-124 <br /> 1.1-Dichloroethene 51.3 2.5 50.0 103 60.9-131 <br /> Trichloroethene 49.2 2.5 50.0 98.4 62.1-126 <br /> Benzene 48.5 2.5 50.0 97.1 65.3-127 <br /> Toluene 46.9 2.5 50.0 93.7 64.3-122 <br /> Surrogate:4-Bromofluotobenzene 50.0 5u.0 100 81.9-128 <br /> Surrogate:Dibromofluoromethane 52.7 50.0 Jos 73-/26 <br /> Surrogate:Toluene-d8 48.5 50.0 96.9 80.4-121 <br /> Matrix Spike(1031037-MSI) Source:T210804-21 Prepared:03/10/21 Analyzed:03/11/21 <br /> Chlorobcnzenc 34.8 2.5 ug/kg 50.0 ND 69.6 65.2-125 QM-07 <br /> 1,1-Dichloroethene 37.0 2.5 50.0 ND 74.0 60.9-131 QM-07 <br /> Trichloroethene 33.8 2.5 50.0 ND 67.5 62.1-126 QM-07 <br /> Benzene 34.1 2.5 50.0 ND 68.2 653-127 QM-07 <br /> Toluene 31.1 2.5 50.0 0.286 61.6 64.3-125 QM-07 <br /> Surrogate:4-Bromojluorobenzene 50.8 520 102 81.9-128 <br /> Surrogate:Dibromofluoromethane 54.3 " <br /> 50.0 109 73-126 <br /> Surrogate:Toluene-d8 48.1 ?0.0 96.5 80.4-121 <br /> Matrix Spike Dup(1031037-MSDI) Source:721080421 Prepared:03/10/21 Analyzed:03/11/21 <br /> Chlorobenzene 34.9 2.5 ug/kg 49.4 ND 70.6 65.2-125 0.120 20 QM-07 <br /> I,1-Dichloroethene 35.8 2.5 :9.4 ND 72.4 60.9-131 3.41 20 QM-07 <br /> Trichloroethene 33.6 2.5 4,).4 ND 68.0 62.1-126 0.455 20 QM-07 <br /> Benzene 34.1 2.5 49.4 ND 69.0 653-127 0.0263 20 QM-07 <br /> Toluene 31.9 2.5 49.4 0.286 64.0 64.3-125 2.59 20 QM-07 <br /> Surrogate:4-Brotnofltmrobenzene 50.1 49.4 101 81.9-128 <br /> Surrogate:Dibromofluoromethane 51.8 49.4 105 73-126 <br /> Surrogate:Toluene-d8 48.4 49.4 98.0 80.4J21 <br /> SunStar Laboratories,Inc. The results in this report apply to the samples analyzed in accordance with the chain at' <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Mike Jaroudi,Project Manager Page 95 of 105 f <br />