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SunStar <br /> 25712 Commercentre Drive <br /> Inc.Laboratories, Lake Forest,California 92630 <br /> 949.297.5020 Phone <br /> lhtovanvr;Qtsv.rry Avtt.vnc:u.Saavicts NarutvwtnFt: 949.297.5027 Fax <br /> WGR Project: NuStar Stockton Terminal <br /> 11021 Winners Circle Suite 101 Project Number: [none] Reported: <br /> Los Alamitos CA,90720 Project Manager: Gray Martz 03/17/21 08:12 <br /> Volatile Organic Compounds by EPA Method 8260B-Quality Control <br /> SunStar Laboratories, Inc. <br /> Reporting Spike Source %REC RPD <br /> .Ane�lvre Result Limit Units Level Result %REC' Limits RPD Limit Notes <br /> Batch 1031037-EPA 5030 GCMS <br /> Blank(1031037-BLlil) Prepared:03/10!21 Analyzed:03/11/21 <br /> p-Isopropyltolucnc ND 2.5 ug/kg <br /> Methylene chloride ND 10 " <br /> Naphthalene ND 2.5 " <br /> n-Propylbcnzcnc ND 2.5 " <br /> Styrene ND 2.5 <br /> 1,1,2,2-1'ctrachloroethane ND 2.5 " <br /> 1,t,1,2-Tetrachloroethane ND 2.5 <br /> Tetrachloroethene ND 2.5 <br /> 1,23-Trichlorobenzene ND 2.5 " <br /> 1,2.4-Trichlorobenzene ND 2.5 " <br /> 1,1,2-Trichloroethane ND 2.5 <br /> 1,1,1-Trichloroethane ND 2.5 <br /> Trichloroethene ND 2.5 " <br /> Trichlorofluoromethane ND 2.5 <br /> 12,3-Trichloropropanc ND 2.5 " <br /> 1,3,5-Trimethyibenzene ND 2.5 f <br /> 1.2,4-Trimethylbenzene ND 2.5 i <br /> Vinyl chloride ND 2.5 <br /> Benzene ND 2.5 1 <br /> Toluene ND 2.5 " <br /> Ethylbenzene ND 2.5 <br /> m,p-Xylene ND 5.0 " <br /> o-Xylenc ND 2.5 " <br /> Tert-amyl methyl ether ND 10 " <br /> Tert-butyl alcohol ND 25 " <br /> Di-isopropyl ether ND l0 " <br /> Ethyl tert-butyl ether ND 10 " <br /> Methyl tcrt-butyl ether ND 10 " <br /> Surrogaie:4-Bromofluorobenzene 51.0 50.0 101 81.9-118 <br /> Surrogate:DibromoJluoromethane 53.9 50.0 108 73-126 <br /> Surrogate:Toluene-d8 48.0 50.0 96.0 80.4-111 <br /> SunStar Laboratories,Inc. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Mike Jaroudi,Project Manager Page 94 of 105 <br />