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SunStar <br /> 25712 Commercentre Drive <br /> - Laboratories, Inc. Lake Forest,California 92630 <br /> Paoviotra Quv.rrr Avat.rru:.u.Sravu rs NA'I'll'iN WIDF: <br /> 949.297.5020 Phone <br /> 949.297.5027 Fax <br /> WGR Project: NuStar Stockton Terminal <br /> 11021 Winners Circle Suite 101 Project Number: [none] Reported: <br /> Los Alamitos CA,90720 Project Manager: Gray Martz 03/17/2108:12 <br /> Volatile Organic Compounds by EPA Method 8260B-Quality Control <br /> SunStar Laboratories,Inc. <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPU Limit Notcs <br /> Batch 1031036-EPA 5030 GCMS <br /> Blank(1031036-BLK1) Prepared&Analyzed:03/10/21 <br /> p-lsopropyltoluene ND 2.5 ug/kg <br /> Methylene chloride ND 10 " <br /> Naphthalene ND 2.5 " <br /> n-Propylbenzene ND 2.5 " <br /> Styrene ND 2.5 " <br /> 1,1,2,2-Tetrachloroethane ND 2.5 <br /> 1,I,I Tetrachloroethane ND 2.5 " <br /> l'etrachloroethene ND 2.5 " <br /> 1,2,3-Trichlorobenzene ND 2.5 " <br /> 1,2,4-Trichlorobenzene ND 2.5 <br /> 1,1,2-Trichloroethane ND 2.5 9 <br /> 1,1,1-Trichloroethane ND 2.5 j <br /> Trichloroethene ND 2.5 " <br /> 1 <br /> Trichlorolluoromethane ND 2.5 y <br /> 1,2,3-Trichloropropane ND 2.5 <br /> 1,3,5-Trimethylbenzene ND 2.5 <br /> 1,2,4-Trimethylbenzene ND 2.5 " <br /> Vinyl chloride ND 2.5 " <br /> Benzene ND 2.5 " <br /> Toluene ND 2.5 " <br /> Ethylbenzene ND 2.5 " <br /> m,p-Xylene ND 5.0 " <br /> o-Xylenc ND 2.5 <br /> Tert-amyl methyl ether ND 10 <br /> Tert-butyl alcohol ND 25 " <br /> Di-isopropyl ether ND 10 " <br /> Ethyl tert-butyl ether ND 10 " <br /> Methyl tert-butyl ether ND 10 <br /> Surrogate:4-Bromof7uorobenzene 53.0 50.0 106 81,9-128 <br /> Surrogate:Dibromofluoromethane 44.4 50.0 88.7 73-126 <br /> Surrogate:Toluene-d8 49.4 50.0 98.7 80.4-121 <br /> SunStar Laboratories,Inc. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Mike 7aroudi,Project Manager Page 91 of 105 <br />