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SunStar 25712 Commercentre Drive <br /> Laboratories, Inc. Lake Forest,California 92630 <br /> 949.297.5020 Phone <br /> Pkcr mitis;puAt.rry A:vAtxttcu.5eKvtces N urn*wme 949.297.5027 Fax <br /> WGR Project: NuStar Stockton Terminal <br /> 11021 Winners Circle Suite 101 Project Number: [none] Reported: <br /> Los Alamitos CA,90720 Project Manager: Gray Martz 03/17/21 08:12 <br /> k"olatile Organic Compounds by EPA Method 8260B-Quality Control <br /> SunStar Laboratories,Inc. <br /> Reporting Spike Source %REC RPD <br /> Analyte Resuli Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 1031036-EPA 5030 GCMS <br /> LCS(1031036-BSI) Prepared&Analyzed:03/10/21 <br /> Chlorobenzene 49.6 2.5 ug/kg 50.0 99.1 65.2-124 <br /> 1.1-Dichloroethene 38.8 2.5 50.0 77.7 60.9-131 <br /> Trichloroethene 51.3 2.5 50.0 103 62.1-126 <br /> Benzene 48.4 2.5 50.0 96.8 65.3-127 <br /> Toluene 48.2 2.5 50.0 96.4 64.3-122 <br /> Surrogate:4-Bromofluorobenzene 55.6 50.0 Ill 81.9-118 <br /> Surrogate:DibromoJluoromediane 41.2 50.0 84.4 73-126 <br /> Surrogate:Toluene-d8 49.7 50.0 99.4 80.4-121 <br /> Matrix Spike(1031036-MSI) Source:T210804-01 Prepared&Analyzed:03/10/21 <br /> Chlorobcnzenc 41.2 2.5 ug/kg 49.5 ND 83.2 65.2-125 <br /> 1,1-Dichloroethene 36.7 2.5 49.5 ND 74.1 60.9-131 <br /> Trichloroethene 45.1 2.5 49.5 ND 91.1 62.1-126 <br /> Benzene 42.9 2.5 49.5 ND 86.6 65.3-127 <br /> Toluene 40.8 2.5 49.5 ND 82.4 64.3-125 <br /> Surrogate:4-Bromofluorobenzene 52.5 49.5 106 81.9-118 <br /> Surrogate.Dibromofluoromethane 42.0 49.5 84.9 73-116 <br /> Surrogate:Toluene-d8 47.8 49.5 96.6 80.4-121 <br /> Matrix Spike Dup(1031036-MSDI) Source:T210804-01 Prepared:03/10/21 Analyzed:03/11/21 <br /> Chlorobcnzenc 41.4 2.5 ug/kg 49.9 ND 83.0 65.2-125 0.506 20 <br /> 1.1-Dichloroethene 42.1 2.5 49.9 ND 84.3 60.9-131 13.7 20 <br /> Trichloroethenc 45.2 2.5 49.9 ND 90.6 62.1-126 0.311 20 <br /> Benzene 48.4 2.5 49.9 ND 97.0 65.3-127 12.1 20 <br /> Toluene 44.7 2.5 49.9 ND 89.7 64.3-125 9.26 20 <br /> Surrogate:4-Bromofluorobenzene 51.1 49.9 103 81.9-128 <br /> Surrogate:Dibromofluoromethane 46.0 49.9 92.2 73-126 <br /> Surrogate:Toluene-d8 49.1 49.9 98.4 80.4-121 <br /> SunStar Laboratories,Inc. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirely. <br /> Mike Jaroudi,Project Manager Page 92 of 105 <br />