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Revised Soil Gas Sampling I w Workplan September 8, 2017 <br />CA ARNG, FMS #24, Stocktch., CA Page 7 <br />The temporary wells will be completed at the surface in well boxes, and tubing will be closed off <br />using a luer lock valve, gas-tight valve, or a fitting for capping the tubing to minimize air intrusion <br />from the surface. Well boxes will be traffic rated and completed 1/4-inch above the existing <br />grade to prevent surface runoff in filtration. <br />SOIL GAS SAMPLING AND ANALYSIS <br />Sampling will be completed during the summer, so rainfall is not expected. Should a significant <br />rain event occur, sampling will not take place less than 5 days following the rainfall and after the <br />frontal system has passed the area. Subsurface conditions will most likely be disturbed during <br />drilling and probe placement/installment. To allow for the subsurface to equilibrate back to <br />representative conditions, the purge volume test, leak test, and soil gas sampling will not be <br />conducted until approximately 1 week after installation. Soil vapor well installation method and <br />equilibration will be recorded in the field log book or field form. <br />All sampling activities, including shroud design, shut-in test, leak test, and purge volume test will <br />be conducted per Advisory, Active Soil Gas Investigations (DTSC, et. al., 2015). Helium will be <br />used as the tracer gas. Flow rates between 100 to 200 milliliters per minute (mL/min) and <br />vacuums less than 100 inches of water will be maintained during purging and sampling to <br />minimize stripping (partitioning of vapors from pore water to soil gas), to prevent ambient air <br />from diluting the soil gas samples, and to reduce variability between contractors. Maintaining <br />these flow rates and vacuums will increase the likelihood that representative samples will be <br />collected. A vacuum gauge will be used between the soil gas sample tubing and the soil gas <br />purging device to verify that 100 inches of water or less is maintained during sampling. During <br />purging, subsurface soil vapor conditions will be field screened using a five-gas meter (oxygen, <br />carbon monoxide, hydrogen sulfide, lower explosive limits [LEL], and VOCs). <br />The analytical laboratory will provide sample collection equipment and sample analysis. <br />Samples will be collected in 1-liter Summa® Canisters, each with a dedicated flow regulator. <br />The field crew will record the pressure upon start and completion of the sampling. Typically, <br />canisters are returned to the stationary laboratory with a slight vacuum. Pressure <br />measurements will be collected using a calibrated pressure gauge, using the same gauge at the <br />laboratory and in the field. Field crews will only rely on canister-dedicated pressure gauges if <br />the gauges are calibrated and working properly. <br />Samples will be analyzed by Environmental Protection Agency (EPA) modified analytical <br />method TO-15 for TPHg and for VOCs. Sorbent tubes will be used to collect samples for <br />analysis of diesel-range organics by EPA 10-17. The tubes will be capped with Swagelok®- <br />type caps and combined Teflon® ferrules, rewrapped in aluminum foil, and placed in a chilled <br />storage container immediately after sampling. <br />A chain of custody form will be completed in the field and will include any relevant problems <br />encountered during sample collection. The starting and ending pressures for passivated <br />stainless-steel canisters should be recorded on the chain of custody form and the field notes. To