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Petroleum Hydrocarbons (TPH, modified EPA 8015, GC/FID) benzene, <br />ethylbenzene, toluene and xylenes (BTEX, EPA method 8020). <br />3.0 OUALITY ASSURANCE PLAN <br />3.1 General Sample Collection and Handling Procedures <br />Proper collection and handling are essential to ensure the quality of <br />a sample. Each sample was collected in a suitable container, preserved <br />correctly for the intended analyses, and stored prior to analysis for <br />no longer than the maximum allowable holding time. Details on the <br />procedure for collection and handling of soil samples to be used on <br />this project can be found in Section 1.0 (Methods). <br />3.2 Sample Identification and Chain-of-Custody Procedures <br />Sample identification and chain-of-custody procedures ensure sample <br />integrity and document sample possession from the time of collection <br />to its ultimate disposal. Each sample container submitted analysis was <br />affixed with a label to identify the job number, date, and time of <br />sample collection, and a sample number unique to that sample. This <br />information, in addition to a description of the sample, field mea- <br />surements made, sampling methodology, names of on-site personnel, and <br />any other pertinent field observations were recorded on the borehole <br />log in the field records. All samples were analyzed by a State- <br />certified laboratory. <br />A chain-of-custody form was used to record possession of the sample <br />from time of collection to ifs arrival at the laboratory. When the <br />samples were shipped, the person in custody of them relinquished the <br />samples by signing the chain-of-custody form and noting the time. The <br />sample-control officer at the laboratory verified sample integrity and <br />confirmed that it was collected in the proper container, preserved <br />correctly, and that there was an adequate volume for analysis. <br />If these conditions were met, the sample was assigned a unique log <br />number for identification throughout analysis and reporting. The log <br />number was recorded on the chain-of-custody form and in the legally- <br />required log book maintained by the laboratory in the laboratory. The <br />sample description, date received, client's name and any other <br />relevant information was also recorded. <br />3.3 Analytical Ouality Assurance <br />In addition to routine calibration of the analytical instruments with <br />standards and blank, the analyst is required to run duplicates and <br />spikes on 10 percent of the analyses to insure an added measure of <br />precision and accuracy. Accuracy is also verified through the follow- <br />ing: <br />1. U.S. Environmental Protection Agency (EPA) and State certifica-