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FRIEDMAN & BRUYA, INC. <br /> ENVIRONMENTAL CHEMISTS <br /> Analysis For PNA Compounds By EPA Method 8270C SIM <br /> Client Sample ID: 5B-10.5.0 Client: Geomatrix Consultants, Inc. <br /> Date Received: 05/24/02 Project: 5011.001 (Roberts Property) <br /> Date Extracted: 06/03/02 Lab ID: 205192-10 1110 <br /> Date Analyzed: 06/07/02 Data File: 060718.D <br /> Matrix: Soil Instrument: GCMS3 <br /> Units: ug/kg (ppb) Operator: YA <br /> Lower Upper <br /> Surrogates: % Recovery Limit Limit <br /> Anthracene-d10 80 43 109 <br /> Benzo(a)anthracene-02 121 65 134 <br /> Concentration: <br /> Compounds: ug/kg (ppb) <br /> Naphthalene <50 <br /> Acenaphthylene X50 <br /> Acenaphthene <50 <br /> Fluorene X50 <br /> Phenanthrene <50 <br /> Anthracene <50 <br /> Fluoranthene <50 <br /> Pyrene <50 <br /> Benz(a)anthracene <50 <br /> Chrysene X50 <br /> Benzo(b)fluoranthene X50 <br /> Benzo(k)fluoranthene X50 <br /> Benzo(a)pyrene X50 <br /> Indeno(1,2,3-cd)pyrene <50 <br /> Dibenzo(a,h)anthracene X50 <br /> Benzo(g,h,i)perylene <50 <br /> Note: The sample was diluted due to high levels of interfering compounds. Detection limits are raised <br /> due to dilution and surrogate recoveries may not be meaningful. <br /> 18 <br />