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FREEDMAN & BRUYA, INC. <br /> ENVIRONMENTAL CHEMISTS <br /> Analysis For PNA Compounds By EPA Method 8270C SIM <br /> Client Sample ID: SB-10-10.0 Client: Geomatrix Consultants, Inc. <br /> Date Received: 05/24/02 Project: 5011.001 (Roberts Property) <br /> Date Extracted: 05/03/42 Lab ID: 205192.11 1110 <br /> Date Analyzed: 05/07/02 Data File: 060717.1) <br /> Matrix: Soil Instrument: GCMS3 <br /> Units: ug/kg (ppb) Operator: YA <br /> Lower Upper <br /> Surrogates: %Recovery Limit Limit <br /> Anthracene-d10 103 43 109 <br /> Benzo(a)anthracene-d12 214 vo 65 134 <br /> Concentration: <br /> Compounds: ug/kg(ppb) <br /> Naphthalene 7,300-- <br /> Acenaphthylene X250 <br /> Acenaphthene 1,700 <br /> Fluorene 4,240 <br /> Phenanthrene 5,500 <br /> Anthracene <250 <br /> Fluoranthene 290 <br /> Pyrene 620 <br /> Benz(a)anthracene 380 <br /> Chrysene 1,000 <br /> Benzo(b)fluoranthene X250 <br /> Benzo(k)fluoranthene <250 <br /> Benzo(a)pyrene <250 <br /> Indeno(1,2,3-cd)pyrene <250 <br /> Dibenzo(a,h)anthracene <250 <br /> Benzo(g,h,i)perylene X250 <br /> Note: The sample was diluted due to high levels of interfering compounds. Detection limits are raised <br /> due to dilution and surrogate recoveries may not be meaningful. <br /> vo-The value reported fell outside the control limits established for this analyte. <br /> 19 <br />