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ParameterValueUnits Method AnalyzedProject Name :Project Number :Parcel 2A211602193.400.400Report Number : 80473Date : 03/02/2012SpikedSampleSample Spike LevelSpikeDup.LevelSpiked SampleValueSpiked SampleValueDuplicatePercent Spiked SampleRecov.Percent Spiked SampleRecov.DuplicateRelativePercentDiff.Percent Spiked SampleRecov.LimitRelativePercentDiff.LimitAnalysis DateQC Report : Matrix Spike/ Matrix Spike DuplicateBLANKTPH as Diesel<50 ug/L M EPA 8015 2/29/121000 1000 996 966 99.6 96.6 3.08 70-130 25BLANKTPH as Diesel<50 ug/L M EPA 8015 3/1/121000 1000 999 1030 99.9 103 3.36 70-130 2580473-01Benzene<0.50 ug/L EPA 8260B 2/28/1240.0 40.0 42.0 39.7 105 99.2 5.62 80-120 2580473-01Diisopropyl ether<0.50 ug/L EPA 8260B 2/28/1239.5 39.5 40.6 40.0 103 101 1.45 80-120 2580473-01Ethyl-tert-butyl ether<0.50 ug/L EPA 8260B 2/28/1240.0 40.0 40.1 39.7 100 99.1 1.04 76.5-120 2580473-01Ethylbenzene<0.50 ug/L EPA 8260B 2/28/1240.0 40.0 43.5 41.2 109 103 5.40 80-120 2580473-01Methyl-t-butyl ether<0.50 ug/L EPA 8260B 2/28/1240.4 40.4 39.7 39.0 98.1 96.6 1.57 69.7-121 2580473-01P + M Xylene<0.50 ug/L EPA 8260B 2/28/1240.0 40.0 41.9 39.6 105 98.9 5.70 76.8-120 2580473-01Tert-Butanol<5.0 ug/L EPA 8260B 2/28/12201 201 201 199 100 99.0 1.01 80-120 252795 2nd Street, Suite 300 Davis, CA 95618 530-297-4800KIFF ANALYTICAL, LLCPage 15 of 23