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ParameterValueUnits Method AnalyzedProject Name :Project Number :Parcel 2A211602193.400.400Report Number : 80473Date : 03/02/2012SpikedSampleSample Spike LevelSpikeDup.LevelSpiked SampleValueSpiked SampleValueDuplicatePercent Spiked SampleRecov.Percent Spiked SampleRecov.DuplicateRelativePercentDiff.Percent Spiked SampleRecov.LimitRelativePercentDiff.LimitAnalysis DateQC Report : Matrix Spike/ Matrix Spike Duplicate80473-01Tert-amyl-methyl ether<0.50 ug/L EPA 8260B 2/28/1239.4 39.4 40.2 40.7 102 103 1.27 78.9-120 2580473-01Toluene<0.50 ug/L EPA 8260B 2/28/1240.0 40.0 44.6 41.7 112 104 6.82 80-120 2580473-02Benzene<0.50 ug/L EPA 8260B 2/28/1240.0 40.0 39.2 38.0 98.0 95.0 3.15 80-120 2580473-02Diisopropyl ether<0.50 ug/L EPA 8260B 2/28/1239.5 39.5 39.7 38.8 100 98.2 2.20 80-120 2580473-02Ethyl-tert-butyl ether<0.50 ug/L EPA 8260B 2/28/1240.0 40.0 41.0 39.9 102 99.6 2.84 76.5-120 2580473-02Ethylbenzene<0.50 ug/L EPA 8260B 2/28/1240.0 40.0 42.5 40.8 106 102 4.20 80-120 2580473-02Methyl-t-butyl ether<0.50 ug/L EPA 8260B 2/28/1240.4 40.4 40.9 40.5 101 100 1.09 69.7-121 2580473-02P + M Xylene<0.50 ug/L EPA 8260B 2/28/1240.0 40.0 41.4 39.6 103 98.9 4.50 76.8-120 2580473-02Tert-Butanol<5.0 ug/L EPA 8260B 2/28/12201 201 200 198 99.5 98.4 1.10 80-120 252795 2nd Street, Suite 300 Davis, CA 95618 530-297-4800KIFF ANALYTICAL, LLCPage 16 of 23