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ParameterValueUnits Method AnalyzedProject Name :Project Number :Parcel 2A211602193.400.400Report Number : 80473Date : 03/02/2012SpikedSampleSample Spike LevelSpikeDup.LevelSpiked SampleValueSpiked SampleValueDuplicatePercent Spiked SampleRecov.Percent Spiked SampleRecov.DuplicateRelativePercentDiff.Percent Spiked SampleRecov.LimitRelativePercentDiff.LimitAnalysis DateQC Report : Matrix Spike/ Matrix Spike Duplicate80473-02Tert-amyl-methyl ether<0.50 ug/L EPA 8260B 2/28/1239.4 39.4 41.5 39.3 105 99.6 5.49 78.9-120 2580473-02Toluene<0.50 ug/L EPA 8260B 2/28/1240.0 40.0 39.9 38.4 99.9 96.0 3.91 80-120 2580473-03Benzene<0.50 ug/L EPA 8260B 2/28/1240.0 40.0 39.6 36.5 99.0 91.4 8.00 80-120 2580473-03Diisopropyl ether<0.50 ug/L EPA 8260B 2/28/1239.5 39.5 42.1 39.7 106 100 5.99 80-120 2580473-03Ethyl-tert-butyl ether<0.50 ug/L EPA 8260B 2/28/1240.0 40.0 44.8 41.8 112 104 7.08 76.5-120 2580473-03Ethylbenzene<0.50 ug/L EPA 8260B 2/28/1240.0 40.0 38.1 35.8 95.3 89.4 6.34 80-120 2580473-03Methyl-t-butyl ether<0.50 ug/L EPA 8260B 2/28/1240.4 40.4 45.4 42.4 112 105 6.72 69.7-121 2580473-03P + M Xylene<0.50 ug/L EPA 8260B 2/28/1240.0 40.0 39.8 37.0 99.4 92.5 7.21 76.8-120 2580473-03Tert-Butanol<5.0 ug/L EPA 8260B 2/28/12201 201 205 197 102 98.0 4.09 80-120 252795 2nd Street, Suite 300 Davis, CA 95618 530-297-4800KIFF ANALYTICAL, LLCPage 17 of 23