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Pennittee: Paul Location: Waterloo Effective Date: Permittee shall SELF-MONITORING SAMPLE PROGRAM Shido, Owner and Advanced GeoEnvironmental, Inc., Consultants Food and Fuel, 3032 E. Waterloo Rd. September 23, 2002 perform the following self-monitoring sample program: Parameter Frequency Type Location (diagram attached) Discharge Limit Analytical Method Flow Continuous Metered 001- Final discharge 5 GPM N/A Lower Explosive Limit (gasoline) Continuous Metered and recorded 001- Final discharge 10% N/A pH Once prior to initial discharge and then once per month Grab, well mixed and representative of reporting period 001- Final discharge 5.0 - 10.0 EPA 150.1 Total Petroleum Hydrocarbons Once prior to initial discharge and then once per month Grab, well mixed and representative of reporting period 001- Final discharge 100 mg/1 EPA 1664 EPA 418.1 Benzene Toluene Ethylbenzene Xylene Once prior to initial discharge and then once per month Grab, well mixed and representative of reporting period 001- Final discharge Total= 4.57 mg/1 Benzene= 0.5 mg/1 EPA 8021 EPA 8260 MTBE Once prior to initial discharge and then once per month Grab, well mixed and representative of reporting period 001- Final discharge Below detection limit < 0.5 1.4/1 EPA 8021 EPA 8260 MDL----- 0.5 1tg/1 Cadmium, Total Chromium, Total Copper, Total Lead, Total Nickel, Total Zinc, Total Once prior to initial discharge and then once per year Grab, well mixed and representative of reporting period 001- Final discharge 2.0 mg/1 5.0 mg/1 6.0 mg/1 2.0 mg/1 5.0 mg/1 7.0 mg/1 EPA 200 Series Total Toxic Organics 40 CFR 413 Once prior to initial discharge and then once per year Grab, well mixed and representative of reporting period 001- Final discharge Total= 4.57 mg/1 Benzene= 0.5 mg/1 EPA 624 and EPA 625 Page 1 of 2