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ADVISORY - ACTIVE SOIL GAS INVESTIGATIONS <br />moisture is high and/or finer-grained materials are present, larger diameter tubing, up to <br />3/4-inch, may also be used. Using larger diameter tubing is less susceptible to plugging <br />by high soil moisture and fine-grained materials. The same soil gas sampling protocols <br />for smaller tubing apply to the larger tubing. The probe tip, probe and probe connectors <br />should all have the same diameter to provide a good seal between the formation and <br />the sampling assembly. The following steps will help ensure a good-quality soil gas <br />sample. <br />Clean, dry tubing should be used at all times. If any moisture or unknown <br />material is present in the tubing prior to insertion, decontaminate or replace the <br />tubing; <br />The bottom-end of the tubing should be attached to a soil gas probe tip. <br />Downhole equipment (probe screens, tie wires, etc.) or drive heads should be <br />free of cutting oils and other contaminants; <br />Metal tubes should not be used to collect hydrogen sulfide samples. Nylaflow®, <br />polyetheretherketone (PEEK), and Teflon® are recommended for soil vapor <br />sampling. Low-density polyethylene (L-D PE) should not be used due to <br />decreased performance relative to other tubing types in both off-gassing of <br />VOCs inherent in the tubing structure (contribution to background) and for <br />decreased contaminant recovery (reactivity). Reduced recovery of naphthalene <br />was observed when using Nylaflow® tubing with small sample sizes. For <br />additional information, see Appendix B; <br />Prior to sampling, an assembled soil gas probe, tip and tubing should be blank <br />tested at a frequency of one analysis per new batch of tubing or material used. <br />Demonstration of equipment cleanliness enhances the quality of soil gas data. <br />The need for blank testing of tubing, probe tips, or an assembled soil gas probe <br />should be evaluated through the DQO process. Demonstrating cleanliness is <br />needed because even new, unused, tubing may be stored inappropriately, such <br />as near fuel sources or exhaust ports. Likewise, probe tips may contain residual <br />oils from the manufacturing process. Some common ways of blank testing are <br />as follows: <br />Coiled Tubing. Spools of tubing can be blank tested by collecting a sample <br />of the dead air within the tubing. The tubing should not be purged prior to <br />sampling and the sampling volume should be less than the dead space <br />within the tubing. The air should be analyzed for site constituents. The air <br />sample from the coiled tubing can be collected by either the field crew or by <br />laboratory personnel prior to taking the tubing to the site. <br />Assembled Soil Gas Probe. A soil gas probe can be assembled and then <br />blank tested prior to insertion into the subsurface. A length of tubing <br />representative of the maximum sampling depth for the site should be cut <br />from the tubing spool and a probe tip attached to one end. Pressure <br />gauges, fittings and valves can also be attached as appropriate. A sample <br />of dead air from the probe should be collected in the same manner as when <br />July 2015 12