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McCampbell Analytical, Inc. <br />"When Quality Counts" <br />1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 <br />http://www.mccampbell.com / E-mail: main@,mccampbell.com <br /> <br />Quality Control Report <br />Client: Yara North America WorkOrder: 2101638 <br />Date Prepared: 01/15/2021 BatchID: 213244 <br />Date Analyzed: 01/15/2021 <br />Extraction Method: 5W3550B <br />Instrument: GC48 <br />Analytical Method: 5W8270C <br />Matrix: Soil <br /> <br />Unit: mg/Kg <br />Project: New Site Pond <br /> <br />Sample ID: MB/LCS/LCSD-213244 <br />QC Summary Report for SW8270C <br />Analyte MB <br />Result <br />MDL RL SPK <br />Val <br />MB SS <br />%REC <br />MB SS <br />Limits <br />1,1-Biphenyl ND 0.00280 0.0130 <br />1,2,4-Trichlorobenzene ND 0.0270 0.250 <br />1,2-Dichlorobenzene ND 0.0330 0.250 <br />1,2-Diphenylhydrazine ND 0.0280 0.250 <br />1,3-Dichlorobenzene ND 0.0350 0.250 <br />1,4-Dichlorobenzene ND 0.0330 0.250 <br />1-Methylnaphthalene ND 0.000420 0.00130 <br />2,4,5-Trichlorophenol ND 0.000760 0.00250 <br />2,4,6-Trichlorophenol ND 0.000820 0.00250 <br />2,4-Dichlorophenol ND 0.000670 0.00130 <br />2,4-Dimethylphenol ND 0.0570 0.250 <br />2,4-Dinitrophenol ND 0.150 0.250 <br />2,4-Dinitrotoluene ND 0.00250 0.0130 <br />2,6-Dinitrotoluene ND 0.00140 0.0130 <br />2-Chloronaphthalene ND 0.0270 0.250 <br />2-Chlorophenol ND 0.00210 0.0130 <br />2-Methylnaphthalene ND 0.000450 0.00130 <br />2-Methylphenol (o-Cresol) ND 0.0360 0.250 <br />2-Nitroaniline ND 0.170 1.20 <br />2-Nitrophenol ND 0.170 1.20 <br />3 & 4-Methylphenol (m,p-Cresol) ND 0.0420 0.250 <br />3,3-Dichlorobenzidine ND 0.00100 0.00250 <br />3-Nitroaniline ND 0.150 1.20 <br />4,6-Dinitro-2-methylphenol ND 0.190 1.20 <br />4-Bromophenyl Phenyl Ether ND 0.0300 0.250 <br />4-Chloro-3-methylphenol ND 0.0310 0.250 <br />4-Chloroaniline ND 0.000970 0.00130 <br />4-Chlorophenyl Phenyl Ether ND 0.0500 0.250 <br />4-Nitroaniline ND 0.190 1.20 <br />4-Nitrophenol ND 0.420 1.20 <br />Acenaphthene ND 0.000530 0.00130 <br />Acenaphthylene ND 0.000370 0.00130 <br />Acetochlor ND 0.0290 0.250 <br />Anthracene ND 0.000950 0.00130 <br />Benzidine ND 0.120 1.20 <br />Benzo (a) anthracene ND 0.00400 0.0130 <br />Benzo (a) pyrene ND 0.000980 0.00250 <br />Benzo (b) fluoranthene ND 0.00140 0.00250 <br />(Cont.) <br />CA ELAP 1644 • NELAP 40330RELAP <br />Page 39 of 51