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McCampbell Analytical, Inc. <br />"When Quality Counts" <br />1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 <br />http://www.mccampbell.com / E-mail: main@mccampbell.com <br /> <br />Quality Control Report <br />Client: Yara North America <br />Date Prepared: 01/15/2021 <br />Date Analyzed: 01/15/2021 <br />Instrument: GC48 <br />Matrix: Soil <br />Project: New Site Pond <br />WorkOrder: 2101638 <br />BatchID: 213244 <br />Extraction Method: 5W3550B <br />Analytical Method: SW8270C <br />Unit: mg/Kg <br />Sample ID: MB/LCS/LCSD-213244 <br />QC Summary Report for SW8270C <br />Analyte MB <br />Result <br />MDL RL SPK <br />Val <br />MB SS <br />VoREC <br />MB SS <br />Limits <br />Benzo (g,h,i) perylene ND 0.00120 0.00250 <br />Benzo (k) fluoranthene ND 0.00110 0.00250 <br />Benzyl Alcohol ND 0.560 1.20 <br />Bis (2-chloroethoxy) Methane ND 0.0270 0.250 <br />Bis (2-chloroethyl) Ether ND 0.000550 0.00130 <br />Bis (2-chloroisopropyl) Ether ND 0.00300 0.0130 <br />Bis (2-ethylhexyl) Adipate ND 0.0480 0.250 <br />Bis (2-ethylhexyl) Phthalate ND 0.00520 0.0250 <br />Butylbenzyl Phthalate ND 0.00360 0.0250 <br />Chrysene ND 0.00130 0.00250 <br />Dibenzo (a,h) anthracene ND 0.00140 0.00250 <br />Dibenzofuran ND 0.0290 0.250 <br />Diethyl Phthalate ND 0.00470 0.0130 <br />Dimethyl Phthalate ND 0.00110 0.00250 <br />Di-n-butyl Phthalate ND 0.00380 0.0130 <br />Di-n-octyl Phthalate ND 0.00660 0.0130 <br />Fluoranthene ND 0.000910 0.00250 <br />Fluorene ND 0.00120 0.00250 <br />Hexachlorobenzene ND 0.00120 0.00250 <br />Hexachlorobutadiene ND 0.000230 0.00130 <br />Hexachlorocyclopentadiene ND 0.520 2.00 <br />Hexachloroethane ND 0.00170 0.0130 <br />Indeno (1,2,3-cd) pyrene ND 0.00300 0.0130 <br />Isophorone ND 0.0480 0.250 <br />Naphthalene ND 0.000280 0.00130 <br />Nitrobenzene ND 0.0490 0.250 <br />N-Nitrosodimethylamine ND 0.180 1.20 <br />N-Nitrosodi-n-propylamine ND 0.0640 0.250 <br />N-Nitrosodiphenylamine ND 0.0240 0.250 <br />Pentachlorophenol ND 0.00600 0.0620 <br />Phenanthrene ND 0.00110 0.00500 <br />Phenol ND 0.00680 0.0500 <br />Pyrene ND 0.00180 0.00250 <br />Pyridine ND 0.0610 0.250 <br />(Cont.) <br />CA ELAP 1644 • NELAP 40330RELAP <br />Page 40 of 51