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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11426-008-SA Date Extracted: 04-19-2018 ICal: PCDDFAL3-12-22-17 Acquired: 04-21-2018
<br />Client ID: SP2-8 Date Received: 04-05-2018 GC Column: DB5MS 2005 WHO TEQ: 2.57
<br />Matrix: Solid Amount: 5.01 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4479 % Solids: 96.02
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.212 - 0.0315
<br />1,2,3,7,8-PeCDD 0.487 - J 0.487 0.0468
<br />1,2,3,4,7,8-HxCDD 0.602 - J 0.0602 0.0503
<br />1,2,3,6,7,8-HxCDD 1.78 - J 0.178 0.0490 Total TCDD 0.491 -J
<br />1,2,3,7,8,9-HxCDD 1.22 - J 0.122 0.0488 Total PeCDD 3.77 -J,M
<br />1,2,3,4,6,7,8-HpCDD 41.4 -0.414 0.0541 Total HxCDD 15.4 -
<br />OCDD 358 -0.107 0.0888 Total HpCDD 79.8 -
<br />2,3,7,8-TCDF 2.47 - F 0.247 0.0243
<br />1,2,3,7,8-PeCDF 0.486 - J 0.0146 0.0285
<br />2,3,4,7,8-PeCDF 1.40 - J 0.420 0.0298
<br />1,2,3,4,7,8-HxCDF 1.67 - J 0.167 0.0255
<br />1,2,3,6,7,8-HxCDF 1.17 - J 0.117 0.0253
<br />2,3,4,6,7,8-HxCDF 0.815 - J 0.0815 0.0279
<br />1,2,3,7,8,9-HxCDF 0.489 - J 0.0489 0.0367 Total TCDF 13.9 -
<br />1,2,3,4,6,7,8-HpCDF 8.92 -0.0892 0.0321 Total PeCDF 10.6 -
<br />1,2,3,4,7,8,9-HpCDF 1.21 - J 0.0121 0.0396 Total HxCDF 13.3 -
<br />OCDF 24.3 -0.00729 0.0843 Total HpCDF 24.3 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 94.2 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 79.9 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 85.6 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 87.6 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 71.6 23.0 - 140
<br />13C-OCDD 64.6 17.0 - 157
<br />13C-2,3,7,8-TCDF 99.0 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 76.0 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 72.3 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 89.4 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 94.9 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 91.4 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 88.6 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 79.0 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 87.5 26.0 - 138
<br />13C-OCDF 64.8 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 86.6 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/25/2018
<br />5172 Hillsdale Circle * El Dorado Hills, CA 95762 * Tel (916) 934-0900 * Fax (916) 934-0999 * www.frontieranalytical.com
<br />4/26/2018
<br />of 000020000012
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