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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11426-009-SA Date Extracted: 04-19-2018 ICal: PCDDFAL3-12-22-17 Acquired: 04-21-2018
<br />Client ID: SP2-9 Date Received: 04-05-2018 GC Column: DB5MS 2005 WHO TEQ: 3.43
<br />Matrix: Solid Amount: 5.00 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4479 % Solids: 93.81
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.165 - 0.0315
<br />1,2,3,7,8-PeCDD 0.809 - J 0.809 0.0468
<br />1,2,3,4,7,8-HxCDD 0.719 - J 0.0719 0.0503
<br />1,2,3,6,7,8-HxCDD 2.06 - J 0.206 0.0490 Total TCDD 0.523 -J
<br />1,2,3,7,8,9-HxCDD 1.67 - J 0.167 0.0488 Total PeCDD 4.41 -J,M
<br />1,2,3,4,6,7,8-HpCDD 46.6 -0.466 0.0541 Total HxCDD 21.4 -
<br />OCDD 309 -0.0927 0.0888 Total HpCDD 90.0 -
<br />2,3,7,8-TCDF 4.32 - F 0.432 0.0243
<br />1,2,3,7,8-PeCDF 0.699 - J 0.0210 0.0285
<br />2,3,4,7,8-PeCDF 1.99 - J 0.597 0.0298
<br />1,2,3,4,7,8-HxCDF 1.96 - J 0.196 0.0255
<br />1,2,3,6,7,8-HxCDF 1.15 - J 0.115 0.0253
<br />2,3,4,6,7,8-HxCDF 1.04 - J 0.104 0.0279
<br />1,2,3,7,8,9-HxCDF 0.505 - J 0.0505 0.0367 Total TCDF 21.8 -M
<br />1,2,3,4,6,7,8-HpCDF 9.07 -0.0907 0.0321 Total PeCDF 15.5 -
<br />1,2,3,4,7,8,9-HpCDF 0.828 - J 0.00828 0.0396 Total HxCDF 15.3 -
<br />OCDF 14.0 -0.00420 0.0843 Total HpCDF 20.5 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 93.1 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 84.6 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 81.2 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 90.3 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 74.0 23.0 - 140
<br />13C-OCDD 62.8 17.0 - 157
<br />13C-2,3,7,8-TCDF 95.3 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 77.4 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 76.2 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 91.7 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 98.8 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 91.5 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 92.0 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 80.0 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 86.6 26.0 - 138
<br />13C-OCDF 67.6 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 85.7 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/25/2018
<br />5172 Hillsdale Circle * El Dorado Hills, CA 95762 * Tel (916) 934-0900 * Fax (916) 934-0999 * www.frontieranalytical.com
<br />4/26/2018
<br />of 000020000013
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