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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11426-012-SA Date Extracted: 04-19-2018 ICal: PCDDFAL3-12-22-17 Acquired: 04-21-2018
<br />Client ID: SP2-12 Date Received: 04-05-2018 GC Column: DB5MS 2005 WHO TEQ: 2.21
<br />Matrix: Solid Amount: 5.01 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4479 % Solids: 93.26
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.199 - 0.0315
<br />1,2,3,7,8-PeCDD ND 0.308 -0.0468
<br />1,2,3,4,7,8-HxCDD 0.444 - J 0.0444 0.0503
<br />1,2,3,6,7,8-HxCDD 1.31 - J 0.131 0.0490 Total TCDD 0.457 -J
<br />1,2,3,7,8,9-HxCDD 0.957 - J 0.0957 0.0488 Total PeCDD 1.40 -J,M
<br />1,2,3,4,6,7,8-HpCDD 25.9 -0.259 0.0541 Total HxCDD 11.1 -
<br />OCDD 225 -0.0675 0.0888 Total HpCDD 50.4 -
<br />2,3,7,8-TCDF 4.13 - F 0.413 0.0243
<br />1,2,3,7,8-PeCDF 0.542 - J 0.0163 0.0285
<br />2,3,4,7,8-PeCDF 2.04 - J 0.612 0.0298
<br />1,2,3,4,7,8-HxCDF 2.32 - J 0.232 0.0255
<br />1,2,3,6,7,8-HxCDF 0.924 - J 0.0924 0.0253
<br />2,3,4,6,7,8-HxCDF 0.986 - J 0.0986 0.0279
<br />1,2,3,7,8,9-HxCDF 0.638 - J 0.0638 0.0367 Total TCDF 19.5 -
<br />1,2,3,4,6,7,8-HpCDF 7.25 -0.0725 0.0321 Total PeCDF 12.5 -
<br />1,2,3,4,7,8,9-HpCDF 0.813 - J 0.00813 0.0396 Total HxCDF 14.0 -
<br />OCDF 15.4 -0.00462 0.0843 Total HpCDF 18.2 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 87.1 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 83.7 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 81.8 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 86.3 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 69.5 23.0 - 140
<br />13C-OCDD 53.7 17.0 - 157
<br />13C-2,3,7,8-TCDF 89.5 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 73.1 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 71.2 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 89.9 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 98.8 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 89.0 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 90.0 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 78.7 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 81.5 26.0 - 138
<br />13C-OCDF 59.1 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 85.3 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/25/2018
<br />5172 Hillsdale Circle * El Dorado Hills, CA 95762 * Tel (916) 934-0900 * Fax (916) 934-0999 * www.frontieranalytical.com
<br />4/26/2018
<br />of 000020000016
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