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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11426-011-SA Date Extracted: 04-19-2018 ICal: PCDDFAL3-12-22-17 Acquired: 04-21-2018
<br />Client ID: SP2-11 Date Received: 04-05-2018 GC Column: DB5MS 2005 WHO TEQ: 1.75
<br />Matrix: Solid Amount: 5.01 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4479 % Solids: 91.92
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.189 - 0.0315
<br />1,2,3,7,8-PeCDD 0.401 - J 0.401 0.0468
<br />1,2,3,4,7,8-HxCDD 0.496 - J 0.0496 0.0503
<br />1,2,3,6,7,8-HxCDD 1.42 - J 0.142 0.0490 Total TCDD ND 0.189
<br />1,2,3,7,8,9-HxCDD 0.911 - J 0.0911 0.0488 Total PeCDD 3.26 -J,M
<br />1,2,3,4,6,7,8-HpCDD 31.0 -0.310 0.0541 Total HxCDD 13.6 -
<br />OCDD 262 -0.0786 0.0888 Total HpCDD 61.4 -
<br />2,3,7,8-TCDF 1.66 -0.166 0.0243
<br />1,2,3,7,8-PeCDF 0.294 - J 0.00882 0.0285
<br />2,3,4,7,8-PeCDF 0.785 - J 0.236 0.0298
<br />1,2,3,4,7,8-HxCDF 0.711 - J 0.0711 0.0255
<br />1,2,3,6,7,8-HxCDF 0.617 - J 0.0617 0.0253
<br />2,3,4,6,7,8-HxCDF 0.612 - J 0.0612 0.0279
<br />1,2,3,7,8,9-HxCDF ND 0.347 -0.0367 Total TCDF 9.31 -
<br />1,2,3,4,6,7,8-HpCDF 6.04 -0.0604 0.0321 Total PeCDF 7.08 -
<br />1,2,3,4,7,8,9-HpCDF 0.628 - J 0.00628 0.0396 Total HxCDF 8.60 -
<br />OCDF 14.0 -0.00420 0.0843 Total HpCDF 15.9 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 99.4 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 102 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 91.3 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 97.4 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 81.3 23.0 - 140
<br />13C-OCDD 72.6 17.0 - 157
<br />13C-2,3,7,8-TCDF 105 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 94.5 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 90.1 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 101 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 110 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 103 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 103 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 93.2 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 101 26.0 - 138
<br />13C-OCDF 77.8 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 93.0 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/25/2018
<br />5172 Hillsdale Circle * El Dorado Hills, CA 95762 * Tel (916) 934-0900 * Fax (916) 934-0999 * www.frontieranalytical.com
<br />4/26/2018
<br />of 000020000015
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