|
EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11455-007-SA Date Extracted: 04-27-2018 ICal: PCDDFAL4-12-20-17 Acquired: 04-30-2018
<br />Client ID: SP3-7 Date Received: 04-12-2018 GC Column: DB5MS 2005 WHO TEQ: 0.823
<br />Matrix: Solid Amount: 5.03 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4492 % Solids: 93.06
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.180 - 0.0273
<br />1,2,3,7,8-PeCDD ND 0.299 -0.0570
<br />1,2,3,4,7,8-HxCDD ND 0.210 -0.0793
<br />1,2,3,6,7,8-HxCDD 1.64 - J 0.164 0.0940 Total TCDD 0.811 -J
<br />1,2,3,7,8,9-HxCDD 0.759 - J 0.0759 0.0823 Total PeCDD ND 0.299
<br />1,2,3,4,6,7,8-HpCDD 28.8 -0.288 0.0842 Total HxCDD 11.1 -
<br />OCDD 232 -0.0696 0.172 Total HpCDD 51.5 -
<br />2,3,7,8-TCDF 0.428 - J 0.0428 0.0269
<br />1,2,3,7,8-PeCDF ND 0.246 -0.0449
<br />2,3,4,7,8-PeCDF ND 0.252 -0.0468
<br />1,2,3,4,7,8-HxCDF 0.458 - J 0.0458 0.0437
<br />1,2,3,6,7,8-HxCDF 0.541 - J 0.0541 0.0417
<br />2,3,4,6,7,8-HxCDF 0.454 - J 0.0454 0.0574
<br />1,2,3,7,8,9-HxCDF ND 0.141 -0.0657 Total TCDF 3.89 -M
<br />1,2,3,4,6,7,8-HpCDF 3.06 - J 0.0306 0.0747 Total PeCDF 1.90 -J
<br />1,2,3,4,7,8,9-HpCDF 0.506 - J 0.00506 0.0883 Total HxCDF 4.59 -J
<br />OCDF 5.74 - J 0.00172 0.170 Total HpCDF 7.36 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 94.7 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 96.6 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 97.4 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 96.8 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 91.2 23.0 - 140
<br />13C-OCDD 82.6 17.0 - 157
<br />13C-2,3,7,8-TCDF 97.1 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 91.3 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 92.9 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 89.0 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 88.6 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 87.8 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 86.5 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 87.7 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 89.3 26.0 - 138
<br />13C-OCDF 81.9 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 88.3 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />5/1/2018 5/1/2018
<br />5172 Hillsdale Circle * El Dorado Hills, CA 95762 * Tel (916) 934-0900 * Fax (916) 934-0999 * www.frontieranalytical.com
<br />of 000022000011
|