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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11455-008-SA Date Extracted: 04-27-2018 ICal: PCDDFAL4-12-20-17 Acquired: 04-30-2018
<br />Client ID: SP3-8 Date Received: 04-12-2018 GC Column: DB5MS 2005 WHO TEQ: 1.34
<br />Matrix: Solid Amount: 5.01 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4492 % Solids: 93.69
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.243 - 0.0273
<br />1,2,3,7,8-PeCDD ND 0.352 -0.0570
<br />1,2,3,4,7,8-HxCDD 0.422 - J 0.0422 0.0793
<br />1,2,3,6,7,8-HxCDD 1.29 - J 0.129 0.0940 Total TCDD ND 0.243
<br />1,2,3,7,8,9-HxCDD 1.00 - J 0.100 0.0823 Total PeCDD ND 0.352
<br />1,2,3,4,6,7,8-HpCDD 32.3 -0.323 0.0842 Total HxCDD 9.74 -
<br />OCDD 267 -0.0801 0.172 Total HpCDD 56.5 -
<br />2,3,7,8-TCDF 1.04 -0.104 0.0269
<br />1,2,3,7,8-PeCDF ND 0.232 -0.0449
<br />2,3,4,7,8-PeCDF 0.654 - J 0.196 0.0468
<br />1,2,3,4,7,8-HxCDF 1.10 - J 0.110 0.0437
<br />1,2,3,6,7,8-HxCDF 0.615 - J 0.0615 0.0417
<br />2,3,4,6,7,8-HxCDF 0.724 - J 0.0724 0.0574
<br />1,2,3,7,8,9-HxCDF ND 0.154 -0.0657 Total TCDF 5.68 -M
<br />1,2,3,4,6,7,8-HpCDF 10.2 -0.102 0.0747 Total PeCDF 6.52 -
<br />1,2,3,4,7,8,9-HpCDF 0.794 - J 0.00794 0.0883 Total HxCDF 11.3 -
<br />OCDF 32.1 -0.00963 0.170 Total HpCDF 29.1 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 87.6 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 88.4 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 92.9 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 88.5 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 84.8 23.0 - 140
<br />13C-OCDD 74.9 17.0 - 157
<br />13C-2,3,7,8-TCDF 90.6 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 83.7 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 84.4 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 83.3 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 81.9 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 82.3 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 82.3 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 82.4 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 84.6 26.0 - 138
<br />13C-OCDF 78.1 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 84.5 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />5/1/2018 5/1/2018
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