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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11455-010-SA Date Extracted: 04-27-2018 ICal: PCDDFAL4-12-20-17 Acquired: 05-01-2018
<br />Client ID: SP3-10 Date Received: 04-12-2018 GC Column: DB5MS 2005 WHO TEQ: 0.492
<br />Matrix: Solid Amount: 5.01 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4492 % Solids: 90.08
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.159 - 0.0273
<br />1,2,3,7,8-PeCDD ND 0.282 -0.0570
<br />1,2,3,4,7,8-HxCDD ND 0.237 -0.0793
<br />1,2,3,6,7,8-HxCDD 0.838 - J 0.0838 0.0940 Total TCDD 0.436 -J
<br />1,2,3,7,8,9-HxCDD 0.589 - J 0.0589 0.0823 Total PeCDD ND 0.282
<br />1,2,3,4,6,7,8-HpCDD 11.2 -0.112 0.0842 Total HxCDD 6.24 -
<br />OCDD 72.6 -0.0218 0.172 Total HpCDD 20.4 -
<br />2,3,7,8-TCDF 0.885 - J 0.0885 0.0269
<br />1,2,3,7,8-PeCDF ND 0.186 -0.0449
<br />2,3,4,7,8-PeCDF ND 0.198 -0.0468
<br />1,2,3,4,7,8-HxCDF 0.366 - J 0.0366 0.0437
<br />1,2,3,6,7,8-HxCDF 0.381 - J 0.0381 0.0417
<br />2,3,4,6,7,8-HxCDF 0.262 - J 0.0262 0.0574
<br />1,2,3,7,8,9-HxCDF ND 0.109 -0.0657 Total TCDF 3.32 -
<br />1,2,3,4,6,7,8-HpCDF 2.17 - J 0.0217 0.0747 Total PeCDF 1.37 -J,M
<br />1,2,3,4,7,8,9-HpCDF 0.367 - J 0.00367 0.0883 Total HxCDF 2.68 -J
<br />OCDF 3.33 - J 0.000999 0.170 Total HpCDF 4.31 -J
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 93.6 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 95.3 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 101 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 96.9 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 91.3 23.0 - 140
<br />13C-OCDD 81.7 17.0 - 157
<br />13C-2,3,7,8-TCDF 98.0 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 90.6 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 92.2 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 90.1 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 91.5 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 89.8 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 87.3 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 86.8 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 89.5 26.0 - 138
<br />13C-OCDF 79.8 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 91.0 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />5/1/2018 5/1/2018
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