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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11455-009-SA Date Extracted: 04-27-2018 ICal: PCDDFAL4-12-20-17 Acquired: 05-01-2018
<br />Client ID: SP3-9 Date Received: 04-12-2018 GC Column: DB5MS 2005 WHO TEQ: 0.731
<br />Matrix: Solid Amount: 5.03 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4492 % Solids: 92.21
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD 0.470 - J 0.470 0.0273
<br />1,2,3,7,8-PeCDD ND 0.223 -0.0570
<br />1,2,3,4,7,8-HxCDD ND 0.170 -0.0793
<br />1,2,3,6,7,8-HxCDD 0.526 - J 0.0526 0.0940 Total TCDD 0.470 -J
<br />1,2,3,7,8,9-HxCDD 0.354 - J 0.0354 0.0823 Total PeCDD 1.69 -J
<br />1,2,3,4,6,7,8-HpCDD 8.05 -0.0805 0.0842 Total HxCDD 3.49 -J
<br />OCDD 57.1 -0.0171 0.172 Total HpCDD 14.6 -
<br />2,3,7,8-TCDF 0.546 - J 0.0546 0.0269
<br />1,2,3,7,8-PeCDF ND 0.179 -0.0449
<br />2,3,4,7,8-PeCDF ND 0.180 -0.0468
<br />1,2,3,4,7,8-HxCDF ND 0.203 -0.0437
<br />1,2,3,6,7,8-HxCDF ND 0.212 - 0.0417
<br />2,3,4,6,7,8-HxCDF ND 0.220 - 0.0574
<br />1,2,3,7,8,9-HxCDF ND 0.235 -0.0657 Total TCDF 1.29 -
<br />1,2,3,4,6,7,8-HpCDF 1.82 - J 0.0182 0.0747 Total PeCDF 1.00 -J
<br />1,2,3,4,7,8,9-HpCDF ND 0.173 -0.0883 Total HxCDF 1.77 -J
<br />OCDF 7.04 - J 0.00211 0.170 Total HpCDF 5.65 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 91.9 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 94.3 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 97.8 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 95.7 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 91.1 23.0 - 140
<br />13C-OCDD 81.5 17.0 - 157
<br />13C-2,3,7,8-TCDF 95.6 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 91.5 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 91.8 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 88.0 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 85.7 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 87.3 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 86.4 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 88.1 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 90.2 26.0 - 138
<br />13C-OCDF 82.4 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 85.7 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />5/1/2018 5/1/2018
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