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QC Sample Results <br /> Client: Union Pacific RR Operations eProcurement Job ID: 440-248216-1 <br /> Project/Site: UPRR-Sludge Bin Stockton- New Profile <br /> Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) <br /> Lab Sample ID: LCSD 440-565589/8 Client Sample ID: Lab Control Sample Dup <br /> Matrix: Waste Prep Type: Total/NA <br /> Analysis Batch: 565589 <br /> Spike LCSD LCSD %Rec. RPD <br /> Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> 1,1,2,2-Tetrachloroethane 1000 1060 ug/Kg 106 55-135 0 25 <br /> 1,1,2-Trichloroethane 1000 1100 ug/Kg 110 65-130 2 20 <br /> 1,1-Dichloroethane 1000 1080 ug/Kg 108 65-130 3 20 <br /> 1,1-Dichloroethene 1000 1140 ug/Kg 114 75-140 7 20 <br /> 1,1-Dichloropropene 1000 1090 ug/Kg 109 70-130 3 20 <br /> 1,2,3-Trichlorobenzene 1000 1110 ug/Kg 111 60-135 13 20 ' <br /> 1,2,3-Trichloropropane 1000 1060 ug/Kg 106 55-130 1 25 <br /> 1,2,4-Trichlorobenzene 1000 1130 ug/Kg 113 65-135 7 20 <br /> 1,2,4-Trimethylbenzene 1000 1130 ug/Kg 113 70-125 2 20 <br /> 1,2-Dibromo-3-Chloropropane 1000 1010 ug/Kg 101 45-135 1 25 <br /> 1,2-Dichlorobenzene 1000 1040 ug/Kg 104 70-120 2 20 <br /> 1,2-Dichloroethane 1000 957 ug/Kg 96 60-145 0 20 <br /> 1,2-Dichloropropane 1000 1110 ug/Kg 111 75-125 0 20 <br /> 1,3,5-Trimethylbenzene 1000 1140 ug/Kg 114 70-125 1 20 <br /> 1,3-Dichlorobenzene 1000 1090 ug/Kg 109 70-125 2 20 <br /> 1,3-Dichloropropane 1000 1010 ug/Kg 101 65-130 4 20 <br /> 1,4-Dichlorobenzene 1000 1090 ug/Kg 109 70-125 2 20 <br /> 2,2-Dichloropropane 1000 1120 ug/Kg 112 60-145 3 25 <br /> 2-Chlorotoluene 1000 1110 ug/Kg 111 70-125 1 20 <br /> 4-Chlorotoluene 1000 1120 ug/Kg 112 70-125 0 20 <br /> Benzene 1000 1110 ug/Kg 111 65-120 1 20 <br /> Bromobenzene 1000 1030 ug/Kg 103 70-120 6 20 <br /> Bromoform 1000 969 ug/Kg 97 50-130 3 25 <br /> Bromomethane 1000 1040 ug/Kg 104 30-140 5 30 <br /> Carbon tetrachloride 1000 1060 ug/Kg 106 65-145 0 20 <br /> Chlorobenzene 1000 1040 ug/Kg 104 70-125 4 20 <br /> Chloroethane 1000 1130 ug/Kg 113 40-140 3 25 <br /> Chloroform 1000 1030 ug/Kg 103 75-130 6 20 <br /> Chloromethane 1000 1020 ug/Kg 102 30-140 3 25 <br /> cis-1,2-Dichloroethene 1000 1090 ug/Kg 109 65-130 1 20 <br /> cis-1,3-Dichloropropene 1000 1040 ug/Kg 104 70-130 5 20 <br /> Dibromomethane 1000 994 ug/Kg 99 65-130 3 20 <br /> Dichlorodifluoromethane 1000 741 ug/Kg 74 10-155 1 30 <br /> Ethylbenzene 1000 1110 ug/Kg 111 80-120 1 20 <br /> Hexachlorobutadiene 1000 1090 ug/Kg 109 60-135 3 20 <br /> Isopropylbenzene 1000 1110 ug/Kg 111 70-125 3 20 <br /> m,p-Xylene 1000 1110 ug/Kg 111 70-125 1 20 <br /> Methylene Chloride 1000 1030 ug/Kg 103 60-140 5 20 <br /> Naphthalene 1000 1060 ug/Kg 106 50-140 11 25 <br /> n-Butylbenzene 1000 1180 ug/Kg 118 70-130 1 20 <br /> N-Propylbenzene 1000 1150 ug/Kg 115 70-130 0 20 <br /> o-Xylene 1000 1090 ug/Kg 109 70-125 2 20 <br /> sec-Butylbenzene 1000 1160 ug/Kg 116 70-125 3 20 <br /> Styrene 1000 1060 ug/Kg 106 70-135 2 20 <br /> tert-Butylbenzene 1000 1110 ug/Kg 111 70-125 3 20 <br /> Tetrachloroethene 1000 1090 ug/Kg 109 65-125 4 20 <br /> Toluene 1000 1110 ug/Kg 111 80-120 4 20 <br /> trans-1,2-Dichloroethene 1000 1080 ug/Kg 108 65-130 2 20 <br /> trans-1,3-Dichloropropene 1000 997 ug/Kg 100 65-135 0 20 <br /> Eurofins TestAmerica, Irvine <br /> Page 14 of 32 8/30/2019 <br />