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QC Sample Results Client: Union Pacific RR Operations eProcurement Job ID: 440-248216-1 Project/Site: UPRR-Sludge Bin Stockton- New Profile Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCSD 440-565589/8 Client Sample ID: Lab Control Sample Dup Matrix: Waste Prep Type: Total/NA Analysis Batch: 565589 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Trichloroethene 1000 1060 ug/Kg 106 70-130 5 20 Trichlorofluoromethane 1000 1010 ug/Kg 101 50-145 5 25 Vinyl chloride 1000 1020 ug/Kg 102 10-120 6 30 1,2-Dibromoethane(EDB) 1000 1050 ug/Kg 105 70-130 5 20 Bromochloromethane 1000 1020 ug/Kg 102 65-125 1 20 Bromodichloromethane 1000 1070 ug/Kg 107 65-135 1 20 ' Dibromochloromethane 1000 1020 ug/Kg 102 65-140 0 20 p-Isopropyltoluene 1000 1130 ug/Kg 113 70-125 1 20 2-Butanone(MEK) 5000 4540 ug/Kg 91 40-145 4 30 LCSD LCSD Surrogate %Recovery Qualifier Limits Toluene-d8(Surr) 93 60-140 4-Bromofluorobenzene(Surr) 90 65-140 Dibromofluoromethane(Surr) 99 55-140 Method: 8270C - Semivolatile Organic Compounds (GC/MS) Lab Sample ID: MB 440-564322/1-A Client Sample ID: Method Blank Matrix: Waste Prep Type: Total/NA Analysis Batch: 564438 Prep Batch: 564322 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,2,4-Trichlorobenzene ND 25 10 mg/Kg 08/20/1912:20 08/20/1921:40 1 1,3-Dichlorobenzene ND 25 10 mg/Kg 08/20/1912:20 08/20/1921:40 1 1,4-Dichlorobenzene ND 25 10 mg/Kg 08/20/1912:20 08/20/1921:40 1 2,4,5-Trichlorophenol ND 50 10 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 2,4,6-Trichlorophenol ND 50 6.0 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 2,4-Dichlorophenol ND 25 6.0 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 2,4-Dimethylphenol ND 25 10 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 2,4-Dinitrophenol ND 100 25 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 2,4-Dinitrotoluene ND 25 6.0 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 2,6-Dinitrotoluene ND 25 8.0 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 2-Chloronaphthalene ND 25 6.0 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 2-Chlorophenol ND 25 6.0 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 2-Methylnaphthalene ND 25 6.0 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 2-Methylphenol ND 25 6.0 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 2-Nitroaniline ND 25 6.0 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 2-Nitrophenol ND 25 10 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 3,3'-Dichlorobenzidine ND 63 12 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 3-Nitroaniline ND 25 10 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 4,6-Dinitro-2-methylphenol ND 32 10 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 4-Bromophenyl phenyl ether ND 25 6.0 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 4-Chloro-3-methylphenol ND 25 6.0 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 4-Chloroaniline ND 25 10 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 4-Chlorophenyl phenyl ether ND 25 7.0 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 3-Methylphenol+4-Methylphenol ND 25 10 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 4-Nitroaniline ND 63 10 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 4-Nitrophenol ND 63 11 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 Acenaphthene ND 25 6.0 mg/Kg 08/20/19 12:20 08/20/19 21:40 1 Eurofins TestAmerica, Irvine Page 15 of 32 8/30/2019