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SAMPLE #1 SAND SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. Collected date/time: 04/29/20 11:20 L1213730 Volatile Organic Compounds (GC/MS) by Method 82608 Result Qualifier MDL RDL Dilution Analysis Batch FpAnalyte mg/kg mg/kg mg/kg date/time 1,2-Dibromo-3-Chloropropane U 0.00780 0.0500 2 05/03/2020 17:23 WG1469977 FTc 1,2-Dibromoethane U 0.00130 0.00500 2 05/03/202017:23 WG1469977 Dibromomethane U 0.00150 0.0100 2 05/03/202017:23 WG1469977 FS 1,2-Dichlorobenzene U 0.000850 0.0100 2 05/03/202017:23 WG1469977 1,3-Dichlorobenzene U 0.00120 0.0100 2 05/03/202017:23 WG1469977 1,4-Dichlorobenzene U 0.00140 0.0100 2 05/03/2020 17:23 WG1469977 [Cn] Dichlorodifluoromethane U 0.00322 0.00500 2 05/03/202017:23 WG1469977 1,1-Dichloroethane U 0.000982 0.00500 2 05/03/202017:23 WG1469977 1,2-Dichloroethane U 0.00130 0.00500 2 05/03/202017:23 WG1469977 1,1-Dichloroethene U 0.00121 0.00500 2 05/03/202017:23 WG1469977 cis-1,2-Dichloroethene U 0.00147 0.00500 2 05/03/202017:23 WG1469977 Fc trans-1,2-Dichloroethene U 0.00208 0.0100 2 05/03/202017:23 WG1469977 1,2-Dichloropropane U 0.00284 0.0100 2 05/03/202017:23 WG1469977 7 1,1-Dichloropropene U 0.00162 0.00500 2 05/03/202017:23 WG1469977 ql 1,3-Dichloropropane U 0.00100 0.0100 2 05/03/202017:23 WG1469977 cis-1,3-Dichloropropene U 0.00151 0.00500 2 05/03/202017:23 WG1469977 FAI trans-1,3-Dichloropropene U 0.00228 0.0100 2 05/03/202017:23 WG1469977 2,2-Dichloropropane U 0.00276 0.00500 2 05/03/202017:23 WG1469977 FSC Di-isopropyl ether U 0.000820 0.00200 2 05/03/202017:23 WG1469977 Ethylbenzene 0.0121 0.00147 0.00500 2 05/03/2020 17:23 WG1469977 Hexachloro-1,3-butadiene U 0.0120 0.0500 2 05/03/2020 17:23 WG1469977 Isopropylbenzene 0.00778 0.000850 0.00500 2 05/03/202017:23 WG1469977 p-Isopropyltoluene 0.0189 0.00510 0.0100 2 05/03/202017:23 WG1469977 2-Butanone(MEK) 0.298 0.127 0.200 2 05/03/202017:23 WG1469977 Methylene Chloride U 0.0133 0.0500 2 05/03/202017:23 WG1469977 4-Methyl-2-pentanone(MIBK) 0.392 0.00456 0.0500 2 05/03/202017:23 WG1469977 Methyl tert-butyl ether U 0.000700 0.00200 2 05/03/202017:23 WG1469977 Naphthalene 1.78 0.00976 0.0250 2 05/03/202017:23 WG1469977 n-Propylbenzene 0.0700 0.00190 0.0100 2 05/03/2020 17:23 WG1469977 Styrene U 0.000458 0.0250 2 05/03/202017:23 WG1469977 1,1,1,2-Tetrachloroethane U 0.00190 0.00500 2 05/03/202017:23 WG1469977 1,1,2,2-Tetrachloroethane U 0.00139 0.00500 2 05/03/202017:23 WG1469977 1,1,2-Trichlorotrifluoroethane U 0.00151 0.00500 2 05/03/202017:23 WG1469977 Tetrachloroethene U 0.00179 0.00500 2 05/03/202017:23 WG1469977 Toluene 0.00810 J 0.00260 0.0100 2 05/03/202017:23 WG1469977 1,2,3-Trichlorobenzene U 0.0147 0.0250 2 05/03/202017:23 WG1469977 1,2,4-Trichlorobenzene U 0.00880 0.0250 2 05/03/202017:23 WG1469977 1,1,1-Trichloroethane U 0.00185 0.00500 2 05/03/202017:23 WG1469977 1,1,2-Trichloroethane U 0.00119 0.00500 2 05/03/202017:23 WG1469977 Trichloroethene U 0.00117 0.00200 2 05/03/202017:23 WG1469977 Trichlorofluoromethane U 0.00165 0.00500 2 05/03/202017:23 WG1469977 1,2,3-Trichloropropane U 0.00324 0.0250 2 05/03/202017:23 WG1469977 1,2,4-Trimethylbenzene 1.83 0.00316 0.0100 2 05/03/2020 17:23 WG1469977 1,2,3-Trim ethyl benzene 0.813 0.00316 0.0100 2 05/03/202017:23 WG1469977 1,3,5-Trim ethyl benzene 0.362 0.00400 0.0100 2 05/03/202017:23 WG1469977 Vinyl chloride U 0.00232 0.00500 2 05/03/202017:23 WG1469977 Xylenes,Total 0.135 0.00176 0.0130 2 05/03/2020 17:23 WG1469977 (S)Toluene-d8 109 75.0-131 05/03/202017.23 WG1469977 (S)4-Bromofluorobenzene 105 67.0-138 05/03/202017.23 WG1469977 (S)1,2-Dich/oroethone-d4 104 70.0-130 05/03/202017.23 WG1469977 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-Patriot Environmental Services MODESTO,CERES CA L1213730 05/05/20 19:35 6 of 56