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SAMPLE #1 SAND SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. Collected date/time: 04/29/20 11:20 L1213730 Semi-Volatile Organic Compounds (GC) by Method 8015 Result Qualifier MDL RDL Dilution Analysis Batch FPAnalyte mg/kg mg/kg mg/kg date/time C12-C22 Hydrocarbons 12200 147 800 200 05/02/2020 08:24 WG1469390 FTc C22-C32 Hydrocarbons 168000 13300 40000 10000 05/02/202010:41 WG1469390 C32-C40 Hydrocarbons 10500 266 800 200 05/02/2020 08:24 WG1469390 FSS (S)o-Terpheny/ 0.000 J7 18.0-148 05/02/202010.41 WG1469390 (S)o-Terpheny/ 0.000 J7 18.0-148 05/02/2020 08:24 WG1469390 4Cn Polychlorinated Biphenyls (GC) by Method 8082 Result Qualifier MDL RDL Dilution Analysis Batch _ Analyte mg/kg mg/kg mg/kg date/time PCB 1016 U 0.0118 0.0340 1 05/02/202012:02 WG1469384 FC]PCB 1221 U 0.0118 0.0340 1 05/02/202012:02 WG1469384 PCB 1232 U 0.0118 0.0340 1 05/02/202012:02 WG1469384 PCB 1242 U 0.0118 0.0340 1 05/02/202012:02 WG1469384 7 ql PCB 1248 U 0.00738 0.0170 1 05/02/202012:02 WG1469384 PCB 1254 U 0.00738 0.0170 1 05/02/202012:02 WG1469384 PCB 1260 U 0.00738 0.0170 1 05/02/202012:02 WG1469384 FAI (S)Decochlorobipheny/ 85.7 10.0-135 05/02/202012:02 WG1469384 (S)Tetroch/oro-m-xylene 72.9 10.0-139 05/02/202012:02 WG1469384 FSC Semi Volatile Organic Compounds (GC/MS) by Method 8270C Result Qualifier MDL RDL Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date/time Acenaphthene 0.901 J 0.270 1.67 50 05/02/202011:18 WG1469414 Acenaphthylene U 0.234 1.67 50 05/02/202011:18 WG1469414 Anthracene 0.832 J 0.297 1.67 50 05/02/202011:18 WG1469414 Benzidine U 3.13 83.5 50 05/02/202011:18 WG1469414 Benzo(a)anthracene U 0.293 1.67 50 05/02/202011:18 WG1469414 Benzo(b)fluoranthene U 0.311 1.67 50 05/02/202011:18 WG1469414 Benzo(k)fluoranthene U 0.296 1.67 50 05/02/202011:18 WG1469414 Benzo(g,h,i)perylene U 0.305 1.67 50 05/02/202011:18 WG1469414 Benzo(a)pyrene U 0.309 1.67 50 05/02/202011:18 WG1469414 Bis(2-ch lorethoxy)methane U 0.500 16.7 50 05/02/202011:18 WG1469414 Bis(2-ch loroethyl)ether U 0.550 16.7 50 05/02/202011:18 WG1469414 2,2-Oxybis(1-Chloropropane) U 0.720 16.7 50 05/02/202011:18 WG1469414 4-Bromophenyl-phenylether U 0.585 16.7 50 05/02/202011:18 WG1469414 2-Chloronaphthalene U 0.293 1.67 50 05/02/2020 11:18 WG1469414 4-Chlorophenyl-phenylether U 0.580 16.7 50 05/02/202011:18 WG1469414 Chrysene U 0.331 1.67 50 05/02/202011:18 WG1469414 Dibenz(a,h)anthracene U 0.462 1.67 50 05/02/202011:18 WG1469414 3,3-Dichlorobenzidine U 0.615 16.7 50 05/02/202011:18 WG1469414 2,4-Dinitrotoluene U 0.477 16.7 50 05/02/202011:18 WG1469414 2,6-Dinitrotoluene U 0.545 16.7 50 05/02/202011:18 WG1469414 Fluoranthene 3.80 0.301 1.67 50 05/02/202011:18 WG1469414 Fluorene 1.15 J 0.271 1.67 50 05/02/202011:18 WG1469414 Hexachlorobenzene U 0.590 16.7 50 05/02/202011:18 WG1469414 Hexachloro-1,3-butadiene U 0.560 16.7 50 05/02/202011:18 WG1469414 Hexachlorocyclopentadiene U 0.875 16.7 50 05/02/2020 11:18 WG1469414 Hexachloroethane U 0.655 16.7 50 05/02/2020 11:18 WG1469414 Indeno(1,2,3-cd)pyrene U 0.471 1.67 50 05/02/202011:18 WG1469414 Isophorone U 0.510 16.7 50 05/02/202011:18 WG1469414 Naphthalene 1.64 J 0.418 1.67 50 05/02/202011:18 WG1469414 Nitrobenzene U 0.580 16.7 50 05/02/202011:18 WG1469414 n-Nitrosodimethyla mine U 2.47 16.7 50 05/02/202011:18 WG1469414 n-Nitrosodiphenylamine U 1.26 16.7 50 05/02/202011:18 WG1469414 n-Nitrosodi-n-propylamine U 0.555 16.7 50 05/02/202011:18 WG1469414 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-Patriot Environmental Services MODESTO,CERES CA L1213730 05/05/20 19:35 7 of 56