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SAMPLE #3 MOTOR OIL SAMPLE RESULTS - 03 ONE LAB.NATIONWIDE. Collected date/time: 04/29/20 11:40 L1213730 Volatile Organic Compounds (GC/MS) by Method 82608 Result Qualifier MDL RDL Dilution Analysis Batch FpAnalyte mg/kg mg/kg mg/kg date/time Bromodichloromethane U 0.290 1.00 400 05/03/2020 04:37 WG1469759 FTc Bromoform U 0.468 10.0 400 05/03/2020 04:37 WG1469759 Bromomethane U J3 0.788 5.00 400 05/03/2020 04:37 WG1469759 FSS n-Butylbenzene 12.5 2.10 5.00 400 05/03/2020 04:37 WG1469759 sec-Butyl benzene 2.21 J 1.15 5.00 400 05/03/2020 04:37 WG1469759 tert-Butylbenzene U 0.780 2.00 400 05/03/2020 04:37 WG1469759 [Cn] Carbon tetrachloride U 0.359 2.00 400 05/03/2020 04:37 WG1469759 Chlorobenzene U 0.0840 1.00 400 05/03/2020 04:37 WG1469759 Chlorodibromomethane U 0.245 1.00 400 05/03/2020 04:37 WG1469759 Chloroethane U 0.680 2.00 400 05/03/2020 04:37 WG1469759 Chloroform U 0.412 1.00 400 05/03/2020 04:37 WG1469759 Fc Chloromethane U 1.74 5.00 400 05/03/2020 04:37 WG1469759 2-Chlorotoluene U 0.346 1.00 400 05/03/2020 04:37 WG1469759 4-Chlorotoluene U 0.180 2.00 400 05/03/202004:37 WG1469759 ql 1,2-Dibromo-3-Chloropropane U 1.56 10.0 400 05/03/2020 04:37 WG1469759 1,2-Dibromoethane U 0.259 1.00 400 05/03/2020 04:37 WG1469759 FAI Dibromomethane U 0.300 2.00 400 05/03/2020 04:37 WG1469759 1,2-Dichlorobenzene U 0.170 2.00 400 05/03/2020 04:37 WG1469759 FSC 1,3-Dichlorobenzene U 0.240 2.00 400 05/03/2020 04:37 WG1469759 1,4-Dichlorobenzene U 0.280 2.00 400 05/03/2020 04:37 WG1469759 Dichlorodifluoromethane U 0.644 1.00 400 05/03/2020 04:37 WG1469759 1,1-Dichloroethane U 0.196 1.00 400 05/03/2020 04:37 WG1469759 1,2-Dichloroethane U 0.260 1.00 400 05/03/2020 04:37 WG1469759 1,1-Dichloroethene U 0.242 1.00 400 05/03/2020 04:37 WG1469759 cis-1,2-Dichloroethene U 0.294 1.00 400 05/03/2020 04:37 WG1469759 trans-1,2-Dichloroethene U 0.416 2.00 400 05/03/2020 04:37 WG1469759 1,2-Dichloropropane U J4 0.568 2.00 400 05/03/2020 04:37 WG1469759 1,1-Dichloropropene U 0.324 1.00 400 05/03/2020 04:37 WG1469759 1,3-Dichloropropane U 0.200 2.00 400 05/03/2020 04:37 WG1469759 cis-1,3-Dichloropropene U 0.303 1.00 400 05/03/2020 04:37 WG1469759 trans-1,3-Dichloropropene U 0.456 2.00 400 05/03/2020 04:37 WG1469759 2,2-Dichloropropane U 0.552 1.00 400 05/03/2020 04:37 WG1469759 Di-isopropyl ether U 0.164 0.400 400 05/03/2020 04:37 WG1469759 Ethylbenzene 26.7 0.295 1.00 400 05/03/2020 04:37 WG1469759 Hexachloro-1,3-butadiene U 2.40 10.0 400 05/03/2020 04:37 WG1469759 Isopropylbenzene 3.17 0.170 1.00 400 05/03/2020 04:37 WG1469759 p-Isopropyltoluene 1.93 J 1.02 2.00 400 05/03/2020 04:37 WG1469759 2-Butanone(MEK) U 25.4 40.0 400 05/03/2020 04:37 WG1469759 Methylene Chloride U 2.66 10.0 400 05/03/2020 04:37 WG1469759 4-Methyl-2-pentanone(MIBK) U 0.912 10.0 400 05/03/2020 04:37 WG1469759 Methyl tert-butyl ether U 0.140 0.400 400 05/03/2020 04:37 WG1469759 Naphthalene 49.0 1.95 5.00 400 05/03/2020 04:37 WG1469759 n-Propylbenzene 18.5 0.380 2.00 400 05/03/2020 04:37 WG1469759 Styrene U J4 0.0916 5.00 400 05/03/2020 04:37 WG1469759 1,1,1,2-Tetrachloroethane U 0.379 1.00 400 05/03/2020 04:37 WG1469759 1,1,2,2-Tetrachloroethane U 0.278 1.00 400 05/03/2020 04:37 WG1469759 1,1,2-Trichlorotrifluoroethane U 0.302 1.00 400 05/03/2020 04:37 WG1469759 Tetrachloroethene U 0.358 1.00 400 05/03/2020 04:37 WG1469759 Toluene 42.3 0.520 2.00 400 05/03/2020 04:37 WG1469759 1,2,3-Trichlorobenzene U 2.93 5.00 400 05/03/2020 04:37 WG1469759 1,2,4-Trichlorobenzene U 1.76 5.00 400 05/03/2020 04:37 WG1469759 1,1,1-Trichloroethane U 0.369 1.00 400 05/03/2020 04:37 WG1469759 1,1,2-Trichloroethane U 0.239 1.00 400 05/03/2020 04:37 WG1469759 Trichloroethene U 0.234 0.400 400 05/03/2020 04:37 WG1469759 Trichlorofluoromethane U 0.331 1.00 400 05/03/2020 04:37 WG1469759 1,2,3-Trichloropropane U 0.648 5.00 400 05/03/2020 04:37 WG1469759 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-Patriot Environmental Services MODESTO,CERES CA L1213730 05/05/20 19:35 14 of 56