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SAMPLE #3 MOTOR OIL SAMPLE RESULTS - 03 ONE LAB.NATIONWIDE. Collected date/time: 04/29/20 11:40 L1213730 Volatile Organic Compounds (GC/MS) by Method 82608 Result Qualifier MDL RDL Dilution Analysis Batch FpAnalyte mg/kg mg/kg mg/kg date/time 1,2,4-Trimethylbenzene 142 0.632 2.00 400 05/03/2020 04:37 WG1469759 FTc 1,2,3-Trim ethyl benzene 48.7 0.632 2.00 400 05/03/2020 04:37 WG1469759 1,3,5-Trim ethyl benzene 33.1 0.800 2.00 400 05/03/2020 04:37 WG1469759 FSS Vinyl chloride U 0.464 1.00 400 05/03/2020 04:37 WG1469759 Xylenes,Total 169 0.352 2.60 400 05/03/2020 04:37 WG1469759 (S)Toluene-d8 106 75.0-131 05/03/2020 0437 WG1469759 [C n (S)4-Bromofluorobenzene 105 67.0-138 05/03/2020 04:37 WG1469759 (S)1,2-Dich/oroethone-d4 95.5 70.0-130 05/03/2020 04:37 WG1469759 Semi-Volatile Organic Compounds (GC) by Method 8015 6 Result Qualifier MDL RDL Dilution Analysis Batch QC Analyte mg/kg mg/kg mg/kg date/time C12-C22 Hydrocarbons 62100 4400 24000 6000 05/02/2020 22:53 WG1469392 GI C22-C32 Hydrocarbons 998000 19900 60000 15000 05/03/202014:15 WG1469392 C32-C40 Hydrocarbons 135000 7980 24000 6000 05/02/2020 22:53 WG1469392 FAI(S)o-Terpheny/ 0.000 J7 18.0-148 05/02/2020 22:53 WG1469392 (S)o-Terpheny/ 0.000 J7 18.0-148 05/03/202014:15 WG1469392 9Sc Semi Volatile Organic Compounds (GC/MS) by Method 8270C Result Qualifier MDL RDL Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date/time Acenaphthene U 32.3 200 6000 05/03/2020 01:48 WG1469417 Acenaphthylene U 28.1 200 6000 05/03/2020 01:48 WG1469417 Anthracene U 35.6 200 6000 05/03/2020 01:48 WG1469417 Benzidine U 376 10000 6000 05/03/2020 01:48 WG1469417 Benzo(a)anthracene U 35.2 200 6000 05/03/2020 01:48 WG1469417 Benzo(b)fluoranthene U 37.3 200 6000 05/03/2020 01:48 WG1469417 Benzo(k)fluoranthene U 35.5 200 6000 05/03/2020 01:48 WG1469417 Benzo(g,h,i)perylene U 36.5 200 6000 05/03/2020 01:48 WG1469417 Benzo(a)pyrene U 37.1 200 6000 05/03/2020 01:48 WG1469417 Bis(2-chlorethoxy)methane U 60.0 2000 6000 05/03/2020 01:48 WG1469417 Bis(2-ch loroethyl)ether U 66.0 2000 6000 05/03/2020 01:48 WG1469417 2,2-Oxybis(1-Chloropropane) U 86.4 2000 6000 05/03/2020 01:48 WG1469417 4-Bromophenyl-phenylether U 70.2 2000 6000 05/03/2020 01:48 WG1469417 2-Chloronaphthalene U 35.1 200 6000 05/03/2020 01:48 WG1469417 4-Chlorophenyl-phenylether U 69.6 2000 6000 05/03/2020 01:48 WG1469417 Chrysene u 39.7 200 6000 05/03/2020 01:48 WG1469417 Dibenz(a,h)anthracene U 55.4 200 6000 05/03/2020 01:48 WG1469417 3,3-Dichlorobenzidine U 73.8 2000 6000 05/03/2020 01:48 WG1469417 2,4-Dinitrotoluene U 57.3 2000 6000 05/03/2020 01:48 WG1469417 2,6-Dinitrotoluene U 65.4 2000 6000 05/03/2020 01:48 WG1469417 Fluoranthene U 36.1 200 6000 05/03/2020 01:48 WG1469417 Fluorene U 32.5 200 6000 05/03/2020 01:48 WG1469417 Hexachlorobenzene U 70.8 2000 6000 05/03/2020 01:48 WG1469417 Hexachloro-1,3-butadiene U 67.2 2000 6000 05/03/2020 01:48 WG1469417 Hexachlorocyclopentadiene U J4 105 2000 6000 05/03/2020 01:48 WG1469417 Hexachloroethane U 78.6 2000 6000 05/03/2020 01:48 WG1469417 Indeno(1,2,3-cd)pyrene U 56.5 200 6000 05/03/2020 01:48 WG1469417 Isophorone U 61.2 2000 6000 05/03/2020 01:48 WG1469417 Naphthalene 151 J 50.2 200 6000 05/03/2020 01:48 WG1469417 Nitrobenzene U 69.6 2000 6000 05/03/2020 01:48 WG1469417 n-Nitrosodimethyla mine U 296 2000 6000 05/03/2020 01:48 WG1469417 n-Nitrosodiphenylamine U 151 2000 6000 05/03/2020 01:48 WG1469417 n-Nitrosodi-n-propylamine U 66.6 2000 6000 05/03/2020 01:48 WG1469417 Phenanthrene U 39.7 200 6000 05/03/2020 01:48 WG1469417 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-Patriot Environmental Services MODESTO,CERES CA L1213730 05/05/20 19:35 15 of 56