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WG1469417 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1213730-03,04 Method Blank (MB) FP1(MB)R3524204-3 05/02/20 22:55 MB Result MB Qualifier MB MDL MB RDL 2 Analyte mg/kg mg/kg mg/kg TC Pyrene U 1.94 9.99 Pyridine U 6.60 99.9 FSS 1,2,4-Trichlorobenzene U 3.12 99.9 4-Chloro-3-m ethyl phenol U 3.24 99.9 rCn 2-Chlorophenol U 3.30 99.9 2-Methylphenol U 3.00 99.9 3&4-Methyl Phenol U 3.12 99.9 FSr 2,4-Dichlorophenol U 2.91 99.9 2,4-Dimethylphenol U 2.61 99.9 4,6-Dinitro-2-methylphenol U 22.7 99.9 2,4-Dinitrophenol U 23.4 99.9 2-Nitrophenol U 3.57 99.9 7G1 4-Nitrophenol U 3.12 99.9 Pentachlorophenol U 2.69 99.9 FAI Phenol U 4.02 99.9 2,4,5-Trichlorophenol U 3.39 99.9 2,4,6-Trichlorophenol U 3.21 99.9 FSC (S)Nitrobenzene-d5 74.0 60.0-140 (S)2-Fluorobiphenyl 83.0 60.0-140 (S)p-Terphenyl-d14 872 60.0-140 (S)Phenol-d5 77.5 60.0-140 (S)2-F/uorophenol 89.5 60.0-140 (S)2,4,6-Tribromophenol 101 60.0-140 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS)R3524204-1 05/02/20 22:16•(LCSD)R3524204-2 05/02/20 22:36 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg % % % % % Acenaphthene 100 82.6 85.3 82.6 85.3 60.0-140 3.22 21 Acenaphthylene 100 84.7 87.0 84.7 87.0 60.0-140 2.68 21 Anthracene 100 78.8 81.1 78.8 81.1 60.0-140 2.88 20 Benzo(a)anthracene 100 83.5 85.4 83.5 85.4 60.0-140 2.25 20 Benzo(b)fluoranthene 100 82.1 80.8 82.1 80.8 60.0-140 1.60 22 Benzo(k)fluoranthene 100 77.8 79.4 77.8 79.4 60.0-140 2.04 23 Benzo(g,h,i)perylene 100 81.5 84.3 81.5 84.3 60.0-140 3.38 21 Benzo(a)pyrene 100 86.9 88.0 86.9 88.0 60.0-140 1.26 21 Bis(2-chlorethoxy)methane 100 77.5 78.6 77.5 78.6 60.0-140 1.41 22 Bis(2-chloroethyl)ether 100 78.5 76.7 78.5 76.7 60.0-140 2.32 28 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-Patriot Environmental Services MODESTO,CERES CA L1213730 05/05/20 19:35 50 of 56