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WG1469417 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1213730-03,04 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) FP1(LCS)R3524204-1 05/02/20 22:16•(LCSD)R3524204-2 05/02/2022:36 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits FTC Analyte mg/kg mg/kg mg/kg % % % % % 2,2-Oxybis(1-Chloropropane) 100 79.6 80.2 79.6 80.2 60.0-140 0.751 27 4-Bromophenyl-phenylether 100 87.5 82.9 87.5 82.9 60.0-140 5.40 20 FSS 2-Chloronaphthalene 100 80.0 83.9 80.0 83.9 60.0-140 4.76 22 4-Chlorophenyl-phenylether 100 86.6 91.3 86.6 91.3 60.0-140 5.28 21 [Cn]Chrysene 100 76.9 78.0 76.9 78.0 60.0-140 1.42 20 Dibenz(a,h)anthracene 100 84.5 85.7 84.5 85.7 60.0-140 1.41 22 2,4-Dinitrotoluene 100 99.8 103 99.8 103 60.0-140 3.16 21 FSr 2,6-Dinitrotoluene 100 90.9 96.7 90.9 96.7 60.0-140 6.18 21 Fluoranthene 100 81.2 82.5 81.2 82.5 60.0-140 1.59 20 Fluorene 100 83.1 85.1 83.1 85.1 60.0-140 2.38 20 Hexachlorobenzene 100 90.0 94.2 90.0 94.2 60.0-140 4.56 20 Hexachloro-1,3-butadiene 100 98.7 98.7 98.7 98.7 60.0-140 0.000 26 7G1 Hexachlorocyclopentadiene 100 40.3 43.9 40.3 43.9 60.0-140 J4 J4 8.55 26 Hexachloroethane 100 86.7 88.8 86.7 88.8 60.0-140 2.39 31 FAI Indeno(1,2,3-cd)pyrene 100 85.5 87.9 85.5 87.9 60.0-140 2.77 21 Isophorone 100 76.6 82.1 76.6 82.1 60.0-140 6.93 21 Naphthalene 100 78.5 81.7 78.5 81.7 60.0-140 4.00 24 FSC Nitrobenzene 100 81.1 82.6 81.1 82.6 60.0-140 1.83 24 n-Nitrosodimethyla mine 100 104 97.8 104 97.8 60.0-140 6.14 31 n-Nitrosodiphenyla mine 100 83.2 84.0 83.2 84.0 60.0-140 0.957 20 n-Nitrosodi-n-propylamine 100 72.9 76.0 72.9 76.0 60.0-140 4.16 23 Phenanthrene 100 81.5 82.0 81.5 82.0 60.0-140 0.612 20 Benzylbutyl phthalate 100 83.6 84.4 83.6 84.4 60.0-140 0.952 20 Bis(2-ethylhexyl)phthalate 100 79.1 80.8 79.1 80.8 60.0-140 2.13 20 Di-n-butyl phthalate 100 82.9 84.1 82.9 84.1 60.0-140 1.44 20 Diethyl phthalate 100 84.0 87.6 84.0 87.6 60.0-140 4.20 20 Dimethyl phthalate 100 83.4 85.7 83.4 85.7 60.0-140 2.72 21 Di-n-octyl phthalate 100 84.7 87.8 84.7 87.8 60.0-140 3.59 21 Pyrene 100 76.6 79.6 76.6 79.6 60.0-140 3.84 21 Pyridine 100 70.6 73.5 70.6 73.5 60.0-140 4.02 40 1,2,4-Trichlorobenzene 100 86.1 89.5 86.1 89.5 60.0-140 3.87 25 4-Chloro-3-methylphenol 100 92.4 90.6 92.4 90.6 60.0-140 1.97 20 2-Chlorophenol 100 86.8 86.5 86.8 86.5 60.0-140 0.346 27 2-Methylphenol 100 88.3 86.3 88.3 86.3 60.0-140 2.29 24 3&4-Methyl Phenol 100 88.9 90.0 88.9 90.0 60.0-140 1.23 24 2,4-Dichlorophenol 100 91.5 90.5 91.5 90.5 60.0-140 1.10 21 2,4-Dimethylphenol 100 97.3 98.3 97.3 98.3 60.0-140 1.02 22 4,6-Dinitro-2-methylphenol 100 91.1 98.7 91.1 98.7 60.0-140 8.01 23 2,4-Dinitrophenol 100 98.7 98.7 98.7 98.7 60.0-140 0.000 30 2-Nitrophenol 100 94.4 96.5 94.4 96.5 60.0-140 2.20 24 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-Patriot Environmental Services MODESTO,CERES CA L1213730 05/05/20 19:35 51 of 56