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QC Sample Results <br />Client: Calgon Carbon Corporation TestAmerica Job ID: 180-73514-7 <br />Project/Site: Carbon Acceptance, 20171212.1 <br />Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued) <br />Lab Sample ID: LCS 180-232169/2-A <br />Matrix: Solid <br />Analysis Batch: 232284 <br />Analyte <br />Spike <br />Added <br />LCS LCS <br />Result Qualifier <br />Client Sample ID: Lab Control Sample <br />Prep Type: Total/NA <br />Prep Batch: 232169 <br />%Rec. <br />Unit D %Rec Limits <br />Acenaphthene 100000 66400 ug/Kg 66 47 _ 104 <br />Acenaphthylene 100000 69500 ug/Kg 70 49 - 114 <br />Anthracene 100000 67200 ug/Kg 67 45 - 112 <br />Benzo[a]anthracene 100000 67400 ug/Kg 67 47 - 110 <br />Benzo[a]pyrene 100000 64000 ug/Kg 64 40 - 112 <br />Benzo[b]fluoranthene 100000 59000 ug/Kg 59 41 - 107 <br />Benzo[g,h,i]perylene 100000 62200 ug/Kg 62 38 - 126 <br />Benzo[k]fluoranthene 100000 62700 ug/Kg 63 40 - 115 <br />Bis(2-chloroethoxy)methane 100000 78400 ug/Kg 78 38 - 105 <br />Bis(2-chloroethyl)ether 100000 79900 ug/Kg 80 35 _ 106 <br />Bis(2-ethylhexyl) phthalate 100000 74700 ug/Kg 75 40 - 117 <br />4-Bromophenyl phenyl ether 100000 65500 ug/Kg 66 47 - 110 <br />Butyl benzyl phthalate 100000 71000 ug/Kg 71 35 - 118 <br />Carbazole 100000 67300 ug/Kg 67 45 _ 114 <br />4-Chloroaniline 100000 70200 ug/Kg 70 25 - 108 <br />4-Chloro-3-methylphenol 100000 83800 ug/Kg 84 40 - 109 <br />2-Chloronaphthalene 100000 68400 ug/Kg 68 46 - 101 <br />2-Chlorophenol 100000 76800 ug/Kg 77 40 - 101 <br />4-Chlorophenyl phenyl ether 100000 75500 ug/Kg 75 47 - 109 <br />Chrysene 100000 67900 ug/Kg 68 46 - 111 <br />Dibenz(a,h)anthracene 100000 63500 ug/Kg 64 39 - 127 <br />Dibenzofuran 100000 71600 ug/Kg 72 46 - 104 <br />1,2-Dichlorobenzene 100000 74100 ug/Kg 74 36 - 101 <br />1,3-Dichlorobenzene 100000 74700 ug/Kg 75 35 - 101 <br />1,4-Dichlorobenzene 100000 73400 ug/Kg 73 36 - 101 <br />3,3'-Dichlorobenzidine 100000 59800 ug/Kg 60 25 _ 122 <br />2,4-Dichlorophenol 100000 75500 ug/Kg 75 47 - 105 <br />Diethyl phthalate 100000 72400 ug/Kg 72 47 - 115 <br />2,4-Dimethylphenol 100000 81500 ug/Kg 81 44 - 105 <br />Dimethyl phthalate 100000 70600 ug/Kg 71 49 - 111 <br />Di-n-butyl phthalate 100000 70400 ug/Kg 70 43 _ 121 <br />4,6-Dinitro-2-methylphenol 200000 138000 ug/Kg 69 24 - 134 <br />2,4-Dinitrophenol 200000 123000 ug/Kg 61 10 - 146 <br />2,4-Dinitrotoluene 100000 74200 ug/Kg 74 45 _ 124 <br />2,6-Dinitrotoluene 100000 76500 ug/Kg 76 40 _ 122 <br />Di-n-octyl phthalate 100000 66100 ug/Kg 66 33 - 129 <br />Fluoranthene 100000 69700 ug/Kg 70 40 - 120 <br />Fluorene 100000 69900 ug/Kg 70 46 _ 109 <br />Hexachlorobenzene 100000 62900 ug/Kg 63 47 - 108 <br />Hexachlorobutadiene 100000 71300 ug/Kg 71 43 - 107 <br />Hexachlorocyclopentadiene 100000 64700 ug/Kg 65 23 - 129 <br />Hexachloroethane 100000 77600 ug/Kg 78 35 - 104 <br />Indeno[1,2,3-cd]pyrene 100000 62500 ug/Kg 62 41 - 125 <br />isophorone 100000 81300 ug/Kg 81 40 - 110 <br />2-Methylnaphthalene 100000 71800 ug/Kg 72 45 - 100 <br />2-Methylphenol 100000 82400 ug/Kg 82 40 - 104 <br />Methylphenol, 3 & 4 100000 85000 ug/Kg 85 40 - 114 <br />Naphthalene 100000 70000 ug/Kg 70 38 - 105 <br />TestAmerica Pittsburgh <br />Page 14 of 20 12/21/2017