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QC Sample Results <br />Client: Calgon Carbon Corporation TestAmerica Job ID: 180-73514-7 <br />Project/Site: Carbon Acceptance, 20171212.1 <br />Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued) <br />Lab Sample ID: LCS 180-232169/2-A <br />Matrix: Solid <br />Analysis Batch: 232284 <br />Analyte <br />Spike <br />Added <br />LCS LCS <br />Result Qualifier <br />Client Sample ID: Lab Control Sample <br />Prep Type: Total/NA <br />Prep Batch: 232169 <br />%Rec. <br />Unit D %Rec Limits <br />2-Nitroaniline 100000 88800 ug/Kg 89 45 - 117 <br />3-Nitroaniline 100000 73700 ug/Kg 74 34 _ 122 <br />4-Nitroaniline 100000 73500 ug/Kg 73 38 _ 123 <br />Nitrobenzene 100000 83500 ug/Kg 84 33- 109 <br />2-Nitrophenol 100000 74400 ug/Kg 74 40- 106 <br />4-Nitrophenol 200000 169000 ug/Kg 84 36 - 127 <br />N-Nitrosodi-n-propylamine 100000 89000 ug/Kg 89 42- 107 <br />N-Nitrosodiphenylamine 100000 66200 ug/Kg 66 44 - 111 <br />2,2'-oxybis[1-chloropropane] 100000 44800 ug/Kg 45 31 _ 111 <br />Pentachlorophenol 200000 117000 ug/Kg 58 17- 122 <br />Phenanthrene 100000 65300 ug/Kg 65 43 - 108 <br />Phenol 100000 83600 ug/Kg 84 41 - 102 <br />Pyrene 100000 66100 ug/Kg 66 41 - 115 <br />1,2,4-Trichlorobenzene 100000 65400 ug/Kg 65 43- 100 <br />2,4,5-Trichlorophenol 100000 72600 ug/Kg 73 42 _ 112 <br />2,4,6-Trichlorophenol 100000 68600 ug/Kg 69 45 - 106 <br />LCS LCS <br />Surrogate %Recovery Qualifier Limits <br />2-Fluorobiphenyl 66 35-105 <br />2-Fluorophenol 78 39-103 <br />Nitrobenzene-d5 86 25-104 <br />Phenol-d5 78 25 - 105 <br />Terphenyl-d14 65 25-127 <br />2,4,6-Tribromophenol 58 35- 124 <br />Method: 6010B - Metals (ICP) <br />Lab Sample ID: MB 180-232226/1-A <br />Matrix: Solid <br />Analysis Batch: 232397 <br />Client Sample ID: Method Blank <br />Prep Type: Total/NA <br />Prep Batch: 232226 <br />Analyte <br />MB MB <br />Result Qualifier RL Unit D Prepared Analyzed Dil Fac <br />Lead ND 1.0 mg/Kg 12/18/17 13:09 12/19/17 12:12 1 <br />Lab Sample ID: LCS 180-232226/2-A <br />Matrix: Solid <br />Analysis Batch: 232397 <br />Analyte <br />Client Sample ID: Lab Control Sample <br />Prep Type: Total/NA <br />Prep Batch: 232226 <br />Spike LCS LCS %Rec. <br />Added Result Qualifier Unit D %Rec Limits <br />Lead <br /> 50.0 48.3 mg/Kg 97 80 - 120 <br />TestAmerica Pittsburgh <br />Page 15 of 20 12/21/2017