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QC Sample Results Client: Calgon Carbon Corporation TestAmerica Job ID: 180-66645-1 Project/Site: Carbon Acceptance, 20170538.1 Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCSD 180-212676/3-A Matrix: Solid Analysis Batch: 212779 Analyte Spike Added LCSD LCSD Result Qualifier Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Prep Batch: 212676 %Rec. RPD Unit D %Rec Limits RPD Limit Acenaphthene 100000 86800 ug/Kg 87 47 - 104 1 40 Acenaphthylene 100000 85200 ug/Kg 85 49 - 114 0 38 Anthracene 100000 81600 ug/Kg 82 45 - 112 1 40 Benzo[a]anthracene 100000 79800 ug/Kg 80 47- 110 1 40 Benzo[a]pyrene 100000 81700 ug/Kg 82 40 - 112 0 40 Benzo[b]fluoranthene 100000 79700 ug/Kg 80 41 -107 0 40 Benzo[g,h,i]perylene 100000 80400 ug/Kg 80 38 - 126 2 40 Benzo[k]fluoranthene 100000 77400 ug/Kg 77 40 - 115 3 40 Bis(2-chloroethoxy)methane 100000 79700 ug/Kg 80 38 - 105 1 36 Bis(2-chloroethyl)ether 100000 76600 ug/Kg 77 35 - 106 1 40 Bis(2-ethylhexyl) phthalate 100000 88400 ug/Kg 88 40- 117 3 40 4-Bromophenyl phenyl ether 100000 87700 ug/Kg 88 47 - 110 4 40 Butyl benzyl phthalate 100000 88700 ug/Kg 89 35- 118 1 40 Carbazole 100000 80500 ug/Kg 81 45 - 114 0 36 4-Chloroaniline 100000 76900 ug/Kg 77 25- 108 0 36 4-Chloro-3-methylphenol 100000 88000 ug/Kg 88 40- 109 3 36 2-Chloronaphthalene 100000 84500 ug/Kg 84 46 - 101 4 40 2-Chlorophenol 100000 83400 ug/Kg 83 40 - 101 4 40 4-Chlorophenyl phenyl ether 100000 85000 ug/Kg 85 47 - 109 2 39 Chrysene 100000 78800 ug/Kg 79 46 - 111 1 39 Dibenz(a,h)anthracene 100000 79800 ug/Kg 80 39 _ 127 1 40 Dibenzofuran 100000 79000 ug/Kg 79 46 - 104 2 38 1,2-Dichlorobenzene 100000 79000 ug/Kg 79 36 - 101 0 40 1,3-Dichlorobenzene 100000 79400 ug/Kg 79 35 - 101 1 40 1,4-Dichlorobenzene 100000 78500 ug/Kg 78 36 - 101 2 40 3,3'-Dichlorobenzidine 100000 83600 ug/Kg 84 25 - 122 1 40 2,4-Dichlorophenol 100000 84600 ug/Kg 85 47 - 105 2 35 Diethyl phthalate 100000 88700 ug/Kg 89 47- 115 0 38 2,4-Dimethylphenol 100000 91400 ug/Kg 91 44 - 105 0 40 Dimethyl phthalate 100000 88800 ug/Kg 89 49- 111 2 37 Di-n-butyl phthalate 100000 91500 ug/Kg 92 43 _ 121 1 38 4,6-Dinitro-2-methylphenol 200000 159000 ug/Kg 79 24 _ 134 1 40 2,4-Dinitrophenol 200000 136000 ug/Kg 68 10 - 146 0 40 2,4-Dinitrotoluene 100000 90500 ug/Kg 91 45 - 124 2 40 2,6-Dinitrotoluene 100000 88200 ug/Kg 88 40 - 122 2 40 Di-n-octyl phthalate 100000 92000 ug/Kg 92 33 - 129 1 40 Fluoranthene 100000 87500 ug/Kg 88 40 _ 120 0 36 Fluorene 100000 78200 ug/Kg 78 46 - 109 0 40 Hexachlorobenzene 100000 95100 ug/Kg 95 47 - 108 0 40 Hexachlorobutadiene 100000 80800 ug/Kg 81 43 - 107 2 39 Hexachlorocyclopentadiene 100000 82300 ug/Kg 82 23 - 129 3 40 Hexachloroethane 100000 78700 ug/Kg 79 35- 104 1 40 Indeno[1,2,3-cdipyrene 100000 80100 ug/Kg 80 41- 125 0 40 lsophorone 100000 84600 ug/Kg 85 40 - 110 0 37 2-Methylnaphthalene 100000 79100 ug/Kg 79 45 _ 100 0 40 2-Methylphenol 100000 80200 ug/Kg 80 40 - 104 0 40 Naphthalene 100000 79400 ug/Kg 79 38 - 105 2 32 2-Nitroaniline 100000 99600 ug/Kg 100 45 - 117 3 40 TestAmerica Pittsburgh Page 16 of 22 6/2/2017