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QC Sample Results <br />Client: Calgon Carbon Corporation TestAmerica Job ID: 180-66645-1 <br />Project/Site: Carbon Acceptance, 20170538.1 <br />Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued) <br />Lab Sample ID: LCSD 180-212676/3-A Client Sample ID: Lab Control Sample Dup <br />Matrix: Solid Prep Type: Total/NA <br />Analysis Batch: 212779 Prep Batch: 212676 <br />Analyte <br />Spike <br />Added <br />LCSD LCSD <br />Result Qualifier Unit D %Rec <br />%Rec. <br />Limits RPD <br />RPD <br />Limit <br />3-Nitroaniline 100000 82800 ug/Kg 83 34 - 122 5 39 <br />4-Nitroaniline 100000 84400 ug/Kg 84 38 - 123 3 40 <br />Nitrobenzene 100000 83700 ug/Kg 84 33 - 109 3 33 <br />2-Nitrophenol 100000 82600 ug/Kg 83 40 - 106 2 39 <br />4-Nitrophenol 200000 204000 ug/Kg 102 36 _ 127 0 40 <br />N-Nitrosodi-n-propylamine 100000 81800 ug/Kg 82 42 - 107 1 40 <br />N-Nitrosodiphenylamine 100000 80800 ug/Kg 81 44 - 111 1 40 <br />2,2'-oxybis[1-chloropropane] 100000 71200 ug/Kg 71 31 _ 111 0 40 <br />Pentachlorophenol 200000 119000 ug/Kg 60 17 _ 122 0 40 <br />Phenanthrene 100000 80500 ug/Kg 81 43 - 108 0 39 <br />Phenol 100000 81900 ug/Kg 82 41 - 102 1 39 <br />Pyrene 100000 84600 ug/Kg 85 41 - 115 2 40 <br />1,2,4-Trichlorobenzene 100000 82700 ug/Kg 83 43 - 100 1 36 <br />2,4,5-Trichlorophenol 100000 81800 ug/Kg 82 42 - 112 3 40 <br />2,4,6-Trichlorophenol 100000 86300 ug/Kg 86 45 - 106 2 40 <br />Methylphenol, 3 &4 100000 83700 ug/Kg 84 40 - 114 2 40 <br />LCSD LCSD <br />Surrogate %Recovery Qualifier Limits <br />2-Fluorobiphenyl 74 35- 105 <br />2-Fluorophenot BO 39- 103 <br />Nitrobenzene-d5 77 25- 104 <br />Phenol-d5 75 25- 105 <br />Terphenyl-d14 68 25 - 127 <br />2,4, 6-Tribromophenol 78 35- 124 <br />Method: 6010B - Metals (ICP) <br />Lab Sample ID: MB 180-212846/1-A <br />Matrix: Solid <br />Analysis Batch: 212982 <br />Client Sample ID: Method Blank <br />Prep Type: Total/NA <br />Prep Batch: 212846 <br />Analyte <br />MB MB <br />Result Qualifier RL Unit D Prepared Analyzed Dil Fac <br />Lead ND 1.0 mg/Kg 05/31/17 17:28 06/01/17 13:20 1 <br />Lab Sample ID: LCS 180-212846/2-A <br />Matrix: Solid <br />Analysis Batch: 212982 <br />Analyte <br />Client Sample ID: Lab Control Sample <br />Prep Type: Total/NA <br />Prep Batch: 212846 <br /> <br />Spike LCS LCS %Rec. <br /> <br />Added Result Qualifier Unit D %Rec Limits <br />Lead <br /> 50.0 47.6 mg/Kg 95 80 - 120 <br />TestAmerica Pittsburgh <br />Page 17 of 22 6/2/2017