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l 1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />M c C a m p b e I l Analytic al, Inc. Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 <br />"When Quality Countsrr http://www.mccampbell.com / E-mail: main@mccampbell.com <br />4,6-Dinitro-2-methylphenol 4.6 5.7 6.25 <br />2,4-Dinitrophenol 0.85 0.97 1.25 <br />(Cont.) <br />CA ELAP 1644 • NELAP 4033ORELAP <br />74 92 20-130 21.7 30 <br />68 77 15-130 12.5 30 <br />Page 72 of 87 <br />QC Summary Report for SW8270C <br />Quality Control Report <br />Client: <br />AdvancedGeo, Inc. <br />WorkOrder: <br />2303N80 <br />Date Prepared: <br />04/05/2023 <br />BatchID: <br />267055 <br />Date Analyzed: <br />04/05/2023 <br />Extraction Method: <br />SW3550B <br />Instrument: <br />GC47 <br />Analytical Method: <br />SW8270C <br />Matrix: <br />Soil <br />Unit: <br />mg/Kg <br />Project: <br />Pilkington <br />Sample ID: <br />MB/LCS/LCSD-267055 <br />4,6-Dinitro-2-methylphenol 4.6 5.7 6.25 <br />2,4-Dinitrophenol 0.85 0.97 1.25 <br />(Cont.) <br />CA ELAP 1644 • NELAP 4033ORELAP <br />74 92 20-130 21.7 30 <br />68 77 15-130 12.5 30 <br />Page 72 of 87 <br />QC Summary Report for SW8270C <br />Analyte <br />LCS <br />Result <br />LCSD <br />Result <br />SPK <br />Val <br />LCS <br />%REC <br />LCSD <br />%REC <br />LCS/LCSD <br />Limits <br />RPD <br />RPD <br />Limit <br />Acenaphthene <br />0.051 <br />0.054 <br />0.062 <br />81 <br />87 <br />60-130 <br />6.22 <br />30 <br />Acenaphthylene <br />0.052 <br />0.055 <br />0.062 <br />83 <br />87 <br />60-130 <br />5.79 <br />30 <br />Acetochlor <br />1.1 <br />1.4 <br />1.25 <br />90 <br />109 <br />60-130 <br />19.5 <br />30 <br />Anthracene <br />0.046 <br />0.056 <br />0.062 <br />74 <br />89 <br />60-130 <br />18.0 <br />30 <br />Benzidine <br />1.6 <br />2.0 <br />6.25 <br />26 <br />32 <br />20-130 <br />20.5 <br />30 <br />Benzo(a)anthracene <br />0.051 <br />0.060 <br />0.062 <br />81 <br />97 <br />70-130 <br />17.4 <br />30 <br />Benzo(a)pyrene <br />0.050 <br />0.061 <br />0.062 <br />80 <br />97 <br />70-130 <br />19.4 <br />30 <br />Benzo (b) fluoranthene <br />0.049 <br />0.058 <br />0.062 <br />78 <br />93 <br />60-130 <br />17.1 <br />30 <br />Benzo (g,h,i) perylene <br />0.049 <br />0.057 <br />0.062 <br />78 <br />91 <br />70-130 <br />15.8 <br />30 <br />Benzo (k) fluoranthene <br />0.050 <br />0.063 <br />0.062 <br />80 <br />101 <br />70-130 <br />23.1 <br />30 <br />Benzyl Alcohol <br />4.8 <br />6.1 <br />6.25 <br />76 <br />97 <br />70-130 <br />23.6 <br />30 <br />1,1 -Biphenyl <br />0.052 <br />0.055 <br />0.062 <br />82 <br />88 <br />60-130 <br />6.68 <br />30 <br />Bis (2-chloroethoxy) Methane <br />1.1 <br />1.4 <br />1.25 <br />91 <br />108 <br />70-130 <br />17.0 <br />30 <br />Bis (2-chloroethyl) Ether <br />0.053 <br />0.061 <br />0.062 <br />85 <br />98 <br />60-130 <br />15.0 <br />30 <br />Bis (2-chloroisopropyl) Ether <br />0.045 <br />0.053 <br />0.062 <br />72 <br />86 <br />60-130 <br />17.4 <br />30 <br />Bis (2-ethylhexyl) Adipate <br />1.3 <br />1.6 <br />1.25 <br />103 <br />128 <br />60-130 <br />21.5 <br />30 <br />Bis (2-ethylhexyl) Phthalate <br />0.065 <br />0.079 <br />0.062 <br />105 <br />126 <br />60-130 <br />18.7 <br />30 <br />4-Bromophenyl Phenyl Ether <br />0.96 <br />1.2 <br />1.25 <br />77 <br />92 <br />60-130 <br />18.6 <br />30 <br />Butylbenzyl Phthalate <br />0.066 <br />0.077 <br />0.062 <br />106 <br />123 <br />60-130 <br />15.1 <br />30 <br />4-Chloroaniline <br />0.034 <br />0.039 <br />0.062 <br />55 <br />63 <br />40-130 <br />13.6 <br />30 <br />4-Chloro-3-methylphenol <br />1.1 <br />1.3 <br />1.25 <br />88 <br />106 <br />70-130 <br />18.4 <br />30 <br />2-Chloronaphthalene <br />1.1 <br />1.1 <br />1.25 <br />86 <br />87 <br />60-130 <br />1.08 <br />30 <br />2 -Chlorophenol <br />0.055 <br />0.067 <br />0.062 <br />89 <br />107 <br />60-130 <br />18.9 <br />30 <br />4-Chlorophenyl Phenyl Ether <br />1.0 <br />1.2 <br />1.25 <br />80 <br />95 <br />70-130 <br />17.3 <br />30 <br />Chrysene <br />0.049 <br />0.061 <br />0.062 <br />79 <br />97 <br />70-130 <br />20.8 <br />30 <br />Dibenzo (a,h) anthracene <br />0.043 <br />0.053 <br />0.062 <br />69,F5 <br />86 <br />70-130 <br />21.4 <br />30 <br />Dibenzofuran <br />0.054 <br />0.057 <br />0.062 <br />87 <br />92 <br />60-130 <br />5.23 <br />30 <br />1,2 -Dichlorobenzene <br />0.92 <br />1.1 <br />1.25 <br />74 <br />88 <br />60-130 <br />17.7 <br />30 <br />1,3 -Dichlorobenzene <br />0.92 <br />1.1 <br />1.25 <br />74 <br />90 <br />60-130 <br />19.7 <br />30 <br />1,4 -Dichlorobenzene <br />0.94 <br />1.1 <br />1.25 <br />75 <br />88 <br />60-130 <br />16.2 <br />30 <br />3,3-Dichlorobenzidine <br />0.033 <br />0.039 <br />0.062 <br />53 <br />63 <br />40-130 <br />17.2 <br />30 <br />2,4-Dichlorophenol <br />0.058 <br />0.069 <br />0.062 <br />93 <br />110 <br />60-130 <br />17.4 <br />30 <br />Diethyl Phthalate <br />0.051 <br />0.054 <br />0.062 <br />82 <br />87 <br />70-130 <br />5.92 <br />30 <br />Dimethyl Phthalate <br />0.054 <br />0.058 <br />0.062 <br />87 <br />93 <br />70-130 <br />7.04 <br />30 <br />2,4 -Dimethylphenol <br />1.1 <br />1.4 <br />1.25 <br />91 <br />109 <br />70-130 <br />17.8 <br />30 <br />Di -n -butyl Phthalate <br />0.055 <br />0.066 <br />0.062 <br />89 <br />106 <br />60-130 <br />17.7 <br />30 <br />4,6-Dinitro-2-methylphenol 4.6 5.7 6.25 <br />2,4-Dinitrophenol 0.85 0.97 1.25 <br />(Cont.) <br />CA ELAP 1644 • NELAP 4033ORELAP <br />74 92 20-130 21.7 30 <br />68 77 15-130 12.5 30 <br />Page 72 of 87 <br />