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l 1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />M c C a m p b e I l Analytic al, Inc. Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 <br />"When Quality Countsrr http://www.mccampbell.com / E-mail: main@mccampbell.com <br />2,4,6 -Trichlorophenol <br />(Cont.) <br />CA ELAP 1644 • NELAP 4033ORELAP <br />0.056 0.058 0.062 89 94 60-130 4.97 30 <br />Page 73 of 87 <br />QC Summary Report for SW8270C <br />Quality Control Report <br />Client: <br />AdvancedGeo, Inc. <br />WorkOrder: <br />2303N80 <br />Date Prepared: <br />04/05/2023 <br />BatchID: <br />267055 <br />Date Analyzed: <br />04/05/2023 <br />Extraction Method: <br />SW3550B <br />Instrument: <br />GC47 <br />Analytical Method: <br />SW8270C <br />Matrix: <br />Soil <br />Unit: <br />mg/Kg <br />Project: <br />Pilkington <br />Sample ID: <br />MB/LCS/LCSD-267055 <br />2,4,6 -Trichlorophenol <br />(Cont.) <br />CA ELAP 1644 • NELAP 4033ORELAP <br />0.056 0.058 0.062 89 94 60-130 4.97 30 <br />Page 73 of 87 <br />QC Summary Report for SW8270C <br />Analyte <br />LCS <br />Result <br />LCSD <br />Result <br />SPK <br />Val <br />LCS <br />%REC <br />LCSD <br />%REC <br />LCS/LCSD <br />Limits <br />RPD <br />RPD <br />Limit <br />2,4-Dinitrotoluene <br />0.056 <br />0.061 <br />0.062 <br />90 <br />98 <br />70-130 <br />8.22 <br />30 <br />2,6-Dinitrotoluene <br />0.057 <br />0.062 <br />0.062 <br />91 <br />99 <br />60-130 <br />8.39 <br />30 <br />Di-n-octyl Phthalate <br />1.1 <br />1.4 <br />1.25 <br />89 <br />112 <br />60-130 <br />23.0 <br />30 <br />1,2-Diphenylhydrazine <br />1.1 <br />1.3 <br />1.25 <br />85 <br />101 <br />60-130 <br />17.2 <br />30 <br />Fluoranthene <br />0.048 <br />0.057 <br />0.062 <br />77 <br />92 <br />70-130 <br />17.1 <br />30 <br />Fluorene <br />0.054 <br />0.064 <br />0.062 <br />86 <br />102 <br />60-130 <br />17.0 <br />30 <br />Hexachlorobenzene <br />0.054 <br />0.064 <br />0.062 <br />86 <br />102 <br />70-130 <br />17.4 <br />30 <br />Hexachlorobutadiene <br />0.054 <br />0.064 <br />0.062 <br />86 <br />102 <br />70-130 <br />17.2 <br />30 <br />Hexachlorocyclopentadiene <br />4.8 <br />5.3 <br />6.25 <br />77 <br />85 <br />60-130 <br />10.0 <br />30 <br />Hexachloroethane <br />0.049 <br />0.059 <br />0.062 <br />79 <br />94 <br />70-130 <br />17.6 <br />30 <br />Indeno (1,2,3 -cd) pyrene <br />0.047 <br />0.056 <br />0.062 <br />75 <br />89 <br />70-130 <br />17.3 <br />30 <br />Isophorone <br />1.1 <br />1.3 <br />1.25 <br />86 <br />106 <br />60-130 <br />20.7 <br />30 <br />1 -Methylnaphthalene <br />0.049 <br />0.059 <br />0.062 <br />78 <br />94 <br />70-130 <br />18.6 <br />30 <br />2 -Methylnaphthalene <br />0.049 <br />0.059 <br />0.062 <br />78 <br />94 <br />70-130 <br />18.7 <br />30 <br />2-Methylphenol (o -Cresol) <br />1.0 <br />1.2 <br />1.25 <br />84 <br />98 <br />60-130 <br />15.9 <br />30 <br />3 & 4-Methylphenol (m,p-Cresol) <br />1.0 <br />1.2 <br />1.25 <br />82 <br />99 <br />60-130 <br />18.6 <br />30 <br />Naphthalene <br />0.048 <br />0.057 <br />0.062 <br />77 <br />92 <br />70-130 <br />17.7 <br />30 <br />2-Nitroaniline <br />6.2 <br />6.5 <br />6.25 <br />100 <br />104 <br />70-130 <br />3.85 <br />30 <br />3-Nitroaniline <br />4.0 <br />3.7 <br />6.25 <br />64 <br />59 <br />50-130 <br />8.16 <br />30 <br />4-Nitroaniline <br />5.6 <br />5.5 <br />6.25 <br />90 <br />88 <br />60-130 <br />1.95 <br />30 <br />Nitrobenzene <br />1.2 <br />1.4 <br />1.25 <br />95 <br />115 <br />60-130 <br />19.5 <br />30 <br />2-Nitrophenol <br />6.1 <br />7.4 <br />6.25 <br />97 <br />118 <br />70-130 <br />19.2 <br />30 <br />4-Nitrophenol <br />5.1 <br />5.9 <br />6.25 <br />82 <br />94 <br />60-130 <br />13.8 <br />30 <br />N-Nitrosodimethylamine <br />4.7 <br />5.5 <br />6.25 <br />75 <br />89 <br />70-130 <br />16.3 <br />30 <br />N-Nitrosodi-n-propylamine <br />1.0 <br />1.2 <br />1.25 <br />80 <br />92 <br />60-130 <br />14.5 <br />30 <br />N-Nitrosodiphenylamine <br />1.1 <br />1.3 <br />1.25 <br />87 <br />104 <br />70-130 <br />18.3 <br />30 <br />Pentachlorophenol <br />0.23 <br />0.28 <br />0.31 <br />74 <br />90 <br />50-130 <br />19.0 <br />30 <br />Phenanthrene <br />0.049 <br />0.058 <br />0.062 <br />78 <br />93 <br />60-130 <br />17.7 <br />30 <br />Phenol <br />0.20 <br />0.24 <br />0.25 <br />81 <br />96 <br />60-130 <br />17.0 <br />30 <br />Pyrene <br />0.053 <br />0.065 <br />0.062 <br />85 <br />105 <br />70-130 <br />21.2 <br />30 <br />Pyridine <br />0.83 <br />0.86 <br />1.25 <br />67 <br />69 <br />60-130 <br />3.13 <br />30 <br />2,3,4,6-Tetrachlorophenol <br />1.1 <br />1.2 <br />1.25 <br />86 <br />93 <br />60-130 <br />8.47 <br />30 <br />1,2,4-Trichlorobenzene <br />1.0 <br />1.2 <br />1.25 <br />82 <br />98 <br />60-130 <br />17.9 <br />30 <br />2,4,5 -Trichlorophenol <br />0.061 <br />0.065 <br />0.062 <br />98 <br />104 <br />60-130 <br />5.86 <br />30 <br />2,4,6 -Trichlorophenol <br />(Cont.) <br />CA ELAP 1644 • NELAP 4033ORELAP <br />0.056 0.058 0.062 89 94 60-130 4.97 30 <br />Page 73 of 87 <br />