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Quality Control Report <br />McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 <br />http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts" <br />Client:AdvancedGeo, Inc. <br />Project:Pilkington <br />Date Analyzed:02/02/2021 <br />Date Prepared:02/02/2021 <br />WorkOrder:2102062 <br />BatchID:214289 <br />Analytical Method:SW8270C <br />Unit:mg/Kg <br />Sample ID:MB/LCS/LCSD-214289 <br />Instrument:GC17 <br />Matrix:Soil <br />Extraction Method:SW3550B <br />QC Summary Report for SW8270C <br />Analyte LCS <br />Result <br />LCSD <br />Result <br />SPK <br />Val <br />LCS <br />%REC <br />LCSD <br />%REC <br />LCS/LCSD <br />Limits <br />RPD RPD <br />Limit <br />1,1-Biphenyl 0.0681 0.0728 0.062 109 117 60-130 6.68 30 <br />1,2,4-Trichlorobenzene 1.12 1.13 1.25 90 91 60-130 0.879 30 <br />1,2-Dichlorobenzene 1.09 1.14 1.25 87 91 60-130 4.87 30 <br />1,2-Diphenylhydrazine 1.17 1.24 1.25 93 100 60-130 6.42 30 <br />1,3-Dichlorobenzene 1.06 1.08 1.25 85 86 60-130 1.80 30 <br />1,4-Dichlorobenzene 1.06 1.10 1.25 84 88 60-130 3.91 30 <br />1-Methylnaphthalene 0.0535 0.0575 0.062 86 92 70-130 7.35 30 <br />2,3,4,6-Tetrachlorophenol 1.11 1.18 1.25 89 95 60-130 6.21 30 <br />2,4,5-Trichlorophenol 0.0674 0.0720 0.062 108 115 60-130 6.61 30 <br />2,4,6-Trichlorophenol 0.0568 0.0631 0.062 91 101 60-130 10.5 30 <br />2,4-Dichlorophenol 0.0564 0.0598 0.062 90 96 60-130 5.80 30 <br />2,4-Dimethylphenol 1.18 1.23 1.25 95 98 70-130 3.83 30 <br />2,4-Dinitrophenol 1.19 1.18 1.25 95 94 15-130 0.628 30 <br />2,4-Dinitrotoluene 0.0731 0.0790 0.062 117 126 70-130 7.82 30 <br />2,6-Dinitrotoluene 0.0698 0.0761 0.062 112 122 60-130 8.67 30 <br />2-Chloronaphthalene 1.18 1.24 1.25 95 99 60-130 4.47 30 <br />2-Chlorophenol 0.0646 0.0711 0.062 103 114 60-130 9.57 30 <br />2-Methylnaphthalene 0.0778 0.0826 0.062 124 132,F2 70-130 5.99 30 <br />2-Methylphenol (o-Cresol)1.16 1.29 1.25 92 103 60-130 11.1 30 <br />2-Nitroaniline 5.28 5.63 6.25 84 90 70-130 6.50 30 <br />2-Nitrophenol 5.39 5.64 6.25 86 90 70-130 4.55 30 <br />3 & 4-Methylphenol (m,p-Cresol)1.17 1.22 1.25 94 98 60-130 4.08 30 <br />3,3-Dichlorobenzidine 0.0350 0.0365 0.062 56 58 40-130 4.38 30 <br />3-Nitroaniline 4.48 4.64 6.25 72 74 50-130 3.40 30 <br />4,6-Dinitro-2-methylphenol 4.96 5.15 6.25 79 82 20-130 3.73 30 <br />4-Bromophenyl Phenyl Ether 1.14 1.21 1.25 91 97 60-130 5.85 30 <br />4-Chloro-3-methylphenol 1.08 1.12 1.25 86 90 70-130 3.69 30 <br />4-Chloroaniline 0.0522 0.0559 0.062 84 89 40-130 6.72 30 <br />4-Chlorophenyl Phenyl Ether 1.11 1.17 1.25 89 93 70-130 4.72 30 <br />4-Nitroaniline 4.56 4.87 6.25 73 78 60-130 6.63 30 <br />4-Nitrophenol 4.84 5.02 6.25 77 80 60-130 3.77 30 <br />Acenaphthene 0.0496 0.0527 0.062 79 84 60-130 6.09 30 <br />Acenaphthylene 0.0749 0.0829 0.062 120 133,F2 60-130 10.1 30 <br />Acetochlor 1.11 1.17 1.25 89 93 60-130 4.76 30 <br />Anthracene 0.0473 0.0515 0.062 76 82 60-130 8.56 30 <br />Benzidine 2.36 2.23 6.25 38 36 20-130 5.49 30 <br />Benzo (a) anthracene 0.0550 0.0607 0.062 88 97 70-130 9.91 30 <br />Benzo (a) pyrene 0.0563 0.0657 0.062 90 105 70-130 15.5 30 <br />CA ELAP 1644 • NELAP 4033ORELAP <br />(Cont.) <br />Page 121 of 154