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Quality Control Report <br />McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 <br />http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts" <br />Client:AdvancedGeo, Inc. <br />Project:Pilkington <br />Date Analyzed:02/02/2021 <br />Date Prepared:02/02/2021 <br />WorkOrder:2102062 <br />BatchID:214289 <br />Analytical Method:SW8270C <br />Unit:mg/Kg <br />Sample ID:MB/LCS/LCSD-214289 <br />Instrument:GC17 <br />Matrix:Soil <br />Extraction Method:SW3550B <br />QC Summary Report for SW8270C <br />Analyte LCS <br />Result <br />LCSD <br />Result <br />SPK <br />Val <br />LCS <br />%REC <br />LCSD <br />%REC <br />LCS/LCSD <br />Limits <br />RPD RPD <br />Limit <br />Benzo (b) fluoranthene 0.0744 0.0854 0.062 119 137,F2 60-130 13.7 30 <br />Benzo (g,h,i) perylene 0.0564 0.0685 0.062 90 110 70-130 19.4 30 <br />Benzo (k) fluoranthene 0.0655 0.0701 0.062 105 112 70-130 6.86 30 <br />Benzyl Alcohol 5.62 5.67 6.25 90 91 70-130 0.824 30 <br />Bis (2-chloroethoxy) Methane 1.06 1.11 1.25 85 89 70-130 4.12 30 <br />Bis (2-chloroethyl) Ether 0.0708 0.0749 0.062 113 120 60-130 5.65 30 <br />Bis (2-chloroisopropyl) Ether 0.0706 0.0736 0.062 113 118 60-130 4.19 30 <br />Bis (2-ethylhexyl) Adipate 1.21 1.36 1.25 97 109 60-130 11.8 30 <br />Bis (2-ethylhexyl) Phthalate 0.0586 0.0797 0.062 94 128 60-130 30.5,F2 30 <br />Butylbenzyl Phthalate 0.0640 0.0750 0.062 102 120 60-130 15.8 30 <br />Chrysene 0.0604 0.0631 0.062 97 101 70-130 4.40 30 <br />Dibenzo (a,h) anthracene 0.0524 0.0617 0.062 84 99 70-130 16.3 30 <br />Dibenzofuran 1.16 1.22 1.25 93 97 60-130 4.37 30 <br />Diethyl Phthalate 0.0651 0.0707 0.062 104 113 70-130 8.34 30 <br />Dimethyl Phthalate 0.0601 0.0657 0.062 96 105 70-130 8.96 30 <br />Di-n-butyl Phthalate 0.0614 0.0713 0.062 98 114 60-130 14.9 30 <br />Di-n-octyl Phthalate 0.0742 0.100 0.062 119 161,F2 60-130 30.0 30 <br />Fluoranthene 0.0595 0.0654 0.062 95 105 70-130 9.44 30 <br />Fluorene 0.0605 0.0654 0.062 97 105 60-130 7.71 30 <br />Hexachlorobenzene 0.0632 0.0653 0.062 101 104 70-130 3.23 30 <br />Hexachlorobutadiene 0.0657 0.0672 0.062 105 108 70-130 2.26 30 <br />Hexachlorocyclopentadiene 5.88 5.83 6.25 94 93 60-130 0.812 30 <br />Hexachloroethane 0.0619 0.0645 0.062 99 103 70-130 4.03 30 <br />Indeno (1,2,3-cd) pyrene 0.0629 0.0740 0.062 101 118 70-130 16.2 30 <br />Isophorone 1.17 1.24 1.25 94 99 60-130 5.68 30 <br />Naphthalene 0.0635 0.0665 0.062 102 106 70-130 4.62 30 <br />Nitrobenzene 1.21 1.26 1.25 97 101 60-130 4.65 30 <br />N-Nitrosodimethylamine 5.62 5.78 6.25 90 93 70-130 2.90 30 <br />N-Nitrosodi-n-propylamine 1.13 1.17 1.25 91 94 60-130 3.39 30 <br />N-Nitrosodiphenylamine 1.19 1.25 1.25 95 100 70-130 5.08 30 <br />Pentachlorophenol 0.312 0.334 0.31 100 107 50-130 6.91 30 <br />Phenanthrene 0.0583 0.0621 0.062 93 99 60-130 6.39 30 <br />Phenol 0.248 0.264 0.25 99 106 60-130 6.33 30 <br />Pyrene 0.0641 0.0689 0.062 103 110 70-130 7.23 30 <br />Pyridine 1.00 1.09 1.25 80 87 60-130 8.50 30 <br />CA ELAP 1644 • NELAP 4033ORELAP <br />(Cont.) <br />Page 122 of 154